Benzoic acid, 3-methoxy-, 4-nitrophenyl ester

Base Information

Chemical Name:Benzoic acid, 3-methoxy-, 4-nitrophenyl ester
CAS No.:36718-85-1
Molecular Formula:C14H11NO5
Molecular Weight:273.24100
Hs Code.:
Mol file:36718-85-1.mol

Synonyms:4-nitrophenyl 3-methoxybenzoate;m-Methoxybenzoesaeure-p-nitrophenylester;m-Anisic acid,4-nitrophenyl ester;(p-Nitrophenyl)-m-anisat;

Suppliers and Price of Benzoic acid, 3-methoxy-, 4-nitrophenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 3-methoxy-, 4-nitrophenyl ester

Chemical Property:

PSA：81.35000
LogP:3.34580

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 3-methoxy-, 4-nitrophenyl ester

There total 2 articles about Benzoic acid, 3-methoxy-, 4-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 586-38-9
3-Methoxybenzoic acid

: 36718-85-1
4-nitrophenyl 3-methoxybenzoate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm00402a011

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1711-05-3
m-anisoyl chloride

: 36718-85-1
4-nitrophenyl 3-methoxybenzoate

Guidance literature:: In 1,4-dioxane;

Reference yield:

: 36718-85-1
4-nitrophenyl 3-methoxybenzoate

: 114095-35-1
2,3-bis(4-hydroxyphenyl)-6-hydroxyindenone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1) THf₂₅ deg C, 6 h; 2) THf, 10 h, 25 deg C

2: 67 percent / MeSO₃H / CH₂Cl₂ / 132 h / 25 °C

3: 75 percent / pyridine hydrochloride / 24 h / 160 °C

With methanesulfonic acid; pyridine hydrochloride; sodium hydride; In dichloromethane;
DOI:10.1021/jm00402a011