1,3-Di-Isopropyl-1,1,3,3-Tetramethyl Disiloxane

Base Information

• Chemical Name: 1,3-Di-Isopropyl-1,1,3,3-Tetramethyl Disiloxane
• CAS No.: 36957-90-1
• Molecular Formula: C10H26OSi2
• Molecular Weight: 218.48400
• Mol file: 36957-90-1.mol

Synonyms:dimethylisopropylsilyl ether;1,1,3,3-tetramethyl-1,3-bis(1-methylethyl)disiloxane;Me2iPrSiOSiiPrMe2;isopropyldimethylsilyl ether;1,3-Diisopropyltetramethyldisiloxan;1,3-diisopropyltetramethyldisiloxane;

Chemical Property of 1,3-Di-Isopropyl-1,1,3,3-Tetramethyl Disiloxane

Chemical Property:

• PSA: 9.23000
• LogP: 4.23320

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Di-Isopropyl-1,1,3,3-Tetramethyl Disiloxane

There total 6 articles about 1,3-Di-Isopropyl-1,1,3,3-Tetramethyl Disiloxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon dioxide (124-38-9,18923-20-1) + dimethyl(propan-2-yl)silane (18209-61-5) → methane (34557-54-5,27936-85-2) + 1,3-diisopropyltetramethyldisiloxane (36957-90-1)

Guidance literature:

With [(POCOP)Ir(H)(acetone)]+[B(C₆F₅)4]-; In C₆D₅Cl; at 23 ℃; for 20h; under 760.051 Torr;

DOI:10.1021/ja305318c

Reference yield:

Ethoxyisopropyldimethylsilan (36850-66-5) → 1,3-diisopropyltetramethyldisiloxane (36957-90-1)

Guidance literature:

With hydrogenchloride; In ethanol;

Reference yield:

1,1,3,3-tetramethyl-1,3-dichlorodisiloxane (2401-73-2) + isopropyllithium (1888-75-1) → 1,3-diisopropyltetramethyldisiloxane (36957-90-1)

Guidance literature:

In diethyl ether; at 0 ℃; for 1.5h;

DOI:10.1016/0022-328X(83)89525-4

upstream raw materials:

Ethoxyisopropyldimethylsilan

n-butyllithium

1,1,3,3-tetramethyl-1,3-dichlorodisiloxane

isopropyllithium

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