4-(Benzyloxy)-2,2-dimethylbutanal

Base Information

Chemical Name:4-(Benzyloxy)-2,2-dimethylbutanal
CAS No.:370555-60-5
Molecular Formula:C13H18O2
Molecular Weight:206.285
Hs Code.:
European Community (EC) Number:836-556-3
Nikkaji Number:J2.121.977K
Mol file:370555-60-5.mol

Synonyms:4-(benzyloxy)-2,2-dimethylbutanal;370555-60-5;2,2-dimethyl-4-phenylmethoxybutanal;2,2-Dimethyl-4-(benzyloxy)butanal;AKOS040813402;EN300-384185;F2147-6416;Z2301244462

Suppliers and Price of 4-(Benzyloxy)-2,2-dimethylbutanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-(Benzyloxy)-2,2-dimethylbutanal

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:206.130679813
Heavy Atom Count:15
Complexity:181

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(CCOCC1=CC=CC=C1)C=O

Technology Process of 4-(Benzyloxy)-2,2-dimethylbutanal

There total 9 articles about 4-(Benzyloxy)-2,2-dimethylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 370555-59-2
4-(benzyloxy)-2,2-dimethylbutan-1-ol

: 370555-60-5
4-(benzyloxy)-2,2-dimethylbutanal

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane;
DOI:10.1021/ol047997l

Reference yield:

: 622-08-2,1201808-31-2
2-Benzyloxyethanol

: 370555-60-5
4-(benzyloxy)-2,2-dimethylbutanal

Guidance literature:: Multi-step reaction with 4 steps

1: I₂; PPh₃; imidazole / toluene

2: 86 percent / n-BuLi; diisopropylamine / tetrahydrofuran / -78 - -10 °C

3: LiAlH₄ / diethyl ether

4: 97 percent / (COCl)2; DMSO; Et₃N / CH₂Cl₂

With 1H-imidazole; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; iodine; dimethyl sulfoxide; triethylamine; diisopropylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; 4: Swern oxidation;
DOI:10.1021/ol047997l

Reference yield:

: 54555-84-9
benzyl iodoethyl ether

: 370555-60-5
4-(benzyloxy)-2,2-dimethylbutanal

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / n-BuLi; diisopropylamine / tetrahydrofuran / -78 - -10 °C

2: LiAlH₄ / diethyl ether

3: 97 percent / (COCl)2; DMSO; Et₃N / CH₂Cl₂

With lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; dimethyl sulfoxide; triethylamine; diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; 3: Swern oxidation;
DOI:10.1021/ol047997l