1,1-Cyclopropanedicarboxylic acid, 2-phenyl-

Base Information

Chemical Name:1,1-Cyclopropanedicarboxylic acid, 2-phenyl-
CAS No.:3709-34-0
Molecular Formula:C11H10O4
Molecular Weight:206.19500
Hs Code.:
Mol file:3709-34-0.mol

Synonyms:2-Phenylcyclopropan-1,1-dicarbonsaeure;2-Phenyl-cyclopropan-dicarbonsaeure-(1,1);1-Phenyl-cyclopropan-dicarbonsaeure-(2.2);1-Phenyl-2.2-dicarboxy-cyclopropan;2-phenyl-1,1-cyclopropanedicarboxylic acid;

Suppliers and Price of 1,1-Cyclopropanedicarboxylic acid, 2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-PHENYLCYCLOPROPANE-1,1-DICARBOXYLIC ACID 95.00%
5MG
$ 505.75

Total 1 raw suppliers

Chemical Property of 1,1-Cyclopropanedicarboxylic acid, 2-phenyl-

Chemical Property:

PSA：74.60000
LogP:1.32950

Purity/Quality:

95% ^*data from raw suppliers

2-PHENYLCYCLOPROPANE-1,1-DICARBOXYLIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,1-Cyclopropanedicarboxylic acid, 2-phenyl-

There total 8 articles about 1,1-Cyclopropanedicarboxylic acid, 2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 6626-84-2
dimethyl 2-benzylidenepropanedioate

: 1774-47-6
trimethylsulfoxonium iodide

: 3709-34-0
2-phenyl-1,1-cyclopropanedicarboxylic acid

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.75h;

dimethyl 2-benzylidenepropanedioate; at 23 ℃;

With potassium hydroxide; In methanol; water; at 0 - 20 ℃; for 22h; Further stages.;
DOI:10.1021/ja8015928

Reference yield:

: 42153-89-9
1-phenyl-2--1-ethanone

: 3709-34-0
2-phenyl-1,1-cyclopropanedicarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / ethanol / 0.5 h / Ambient temperature

2: toluenesulfonic acid / benzene / 12 h / Heating

3: 77 percent / NaH / tetrahydrofuran / 5 h / 60 °C

With sodium tetrahydroborate; o-toluenesulfonic acid; sodium hydride; In tetrahydrofuran; ethanol; benzene;
DOI:10.1021/jo01290a012

Reference yield:

: 72174-68-6
S-methyl-S-(trans-2-phenylethenyl)-N-(p-tolylsulfonyl)sulfoximine

: 3709-34-0
2-phenyl-1,1-cyclopropanedicarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / NaH / tetrahydrofuran / 5 h / 60 °C

With sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo01290a012