Carbamic acid, (2-naphthalenylmethyl)-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, (2-naphthalenylmethyl)-, 1,1-dimethylethyl ester
CAS No.:371247-56-2
Molecular Formula:C16H19NO2
Molecular Weight:257.332
Hs Code.:
DSSTox Substance ID:DTXSID70466598
Nikkaji Number:J1.826.564H
Wikidata:Q82293191
Mol file:371247-56-2.mol

Synonyms:371247-56-2;tert-Butyl (naphthalen-2-ylmethyl)carbamate;tert-butyl N-[(naphthalen-2-yl)methyl]carbamate;Carbamic acid, (2-naphthalenylmethyl)-, 1,1-dimethylethyl ester;DTXSID70466598

Suppliers and Price of Carbamic acid, (2-naphthalenylmethyl)-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Carbamic acid, (2-naphthalenylmethyl)-, 1,1-dimethylethyl ester

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:257.141578849
Heavy Atom Count:19
Complexity:308

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NCC1=CC2=CC=CC=C2C=C1

Technology Process of Carbamic acid, (2-naphthalenylmethyl)-, 1,1-dimethylethyl ester

There total 3 articles about Carbamic acid, (2-naphthalenylmethyl)-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 479423-32-0
tert-butyl (naphthalen-2-yl(phenylsulfonyl)methyl)carbamate

: 124-38-9,18923-20-1
carbon dioxide

: 33741-79-6,93779-36-3
Dl-2-t-butoxycarbonylamino-2-(2-naphthyl)-acetic acid

: 371247-56-2
tert-butyl ester [(2-naphthyl)methyl]-carbamic acid

Guidance literature:: tert-butyl (naphthalen-2-yl(phenylsulfonyl)methyl)carbamate; With trimethylsilyltributyltin; cesium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h; Inert atmosphere;

carbon dioxide; In N,N-dimethyl-formamide; at 100 ℃; for 3h; under 7500.75 Torr; Autoclave;

With hydrogenchloride; In diethyl ether; water; N,N-dimethyl-formamide; pH=2; Inert atmosphere;
DOI:10.1002/anie.201006422

Reference yield:

: 4248-19-5
tert-butyl carbazate

: 33741-79-6,93779-36-3
Dl-2-t-butoxycarbonylamino-2-(2-naphthyl)-acetic acid

: 371247-56-2
tert-butyl ester [(2-naphthyl)methyl]-carbamic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: formic acid / methanol; water / 60 h / 20 °C / Inert atmosphere

2.1: trimethylsilyltributyltin; cesium fluoride / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere

2.2: 3 h / 100 °C / 7500.75 Torr / Autoclave

2.3: pH 2 / Inert atmosphere

With formic acid; trimethylsilyltributyltin; cesium fluoride; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201006422

Reference yield:

: 66-99-9
β-naphthaldehyde

: 33741-79-6,93779-36-3
Dl-2-t-butoxycarbonylamino-2-(2-naphthyl)-acetic acid

: 371247-56-2
tert-butyl ester [(2-naphthyl)methyl]-carbamic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: formic acid / methanol; water / 60 h / 20 °C / Inert atmosphere

2.1: trimethylsilyltributyltin; cesium fluoride / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere

2.2: 3 h / 100 °C / 7500.75 Torr / Autoclave

2.3: pH 2 / Inert atmosphere

With formic acid; trimethylsilyltributyltin; cesium fluoride; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201006422