[(3Z)-1-methyl-1-oxido-3H-1lambda~4~,2-benzothiazol-3-ylidene]cyanamide

Base Information

• Chemical Name: [(3Z)-1-methyl-1-oxido-3H-1lambda~4~,2-benzothiazol-3-ylidene]cyanamide
• CAS No.: 58099-00-6
• Molecular Formula: C₉H₇N₃OS
• Molecular Weight: 205.24
• Mol file: 58099-00-6.mol

Synonyms:

Chemical Property of [(3Z)-1-methyl-1-oxido-3H-1lambda~4~,2-benzothiazol-3-ylidene]cyanamide

Chemical Property:

• Vapor Pressure: 3.62E-06mmHg at 25°C
• Boiling Point: 386.1°C at 760 mmHg
• Flash Point: 187.3°C
• Density: 1.37g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(3Z)-1-methyl-1-oxido-3H-1lambda~4~,2-benzothiazol-3-ylidene]cyanamide

There total 5 articles about [(3Z)-1-methyl-1-oxido-3H-1lambda~4~,2-benzothiazol-3-ylidene]cyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methanesulfinyl-benzamide (54705-22-5) → 3-cyanoimino-1-methyl-3H-1λ4-benzo[d]isothiazole 1-oxide (58099-00-6)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. H₃PO₄, P₂O₅, NaN₃

2: CHCl₃ / Heating

With sodium azide; phosphoric acid; phosphorus pentoxide; In chloroform;

Reference yield:

2-methanesulfinyl-benzonitrile (22912-53-4,55715-60-1) → 3-cyanoimino-1-methyl-3H-1λ4-benzo[d]isothiazole 1-oxide (58099-00-6)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. H₃PO₄, P₂O₅, NaN₃

2: CHCl₃ / Heating

With sodium azide; phosphoric acid; phosphorus pentoxide; In chloroform;

Reference yield:

2-methylsulfanyl-benzamide (54705-16-7) → 3-cyanoimino-1-methyl-3H-1λ4-benzo[d]isothiazole 1-oxide (58099-00-6)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. H₂O₂

2: aq. H₃PO₄, P₂O₅, NaN₃

3: CHCl₃ / Heating

With sodium azide; phosphoric acid; dihydrogen peroxide; phosphorus pentoxide; In chloroform;

upstream raw materials:

1-methyl-1-oxo-1λ⁶-benzo[d]isothiazol-3-ylideneamine

bromocyane

CYANAMID

2-methanesulfinyl-benzamide