1,2-Cyclohexanediol, acetate benzoate, cis-

Base Information

Chemical Name:1,2-Cyclohexanediol, acetate benzoate, cis-
CAS No.:37844-64-7
Molecular Formula:C₁₅H₁₈O₄
Molecular Weight:262.306
Hs Code.:
Mol file:37844-64-7.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Cyclohexanediol, acetate benzoate, cis-

Chemical Property:

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Technology Process of 1,2-Cyclohexanediol, acetate benzoate, cis-

There total 3 articles about 1,2-Cyclohexanediol, acetate benzoate, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37854-36-7,59694-07-4,86703-61-9,86703-62-0,120053-18-1,72375-13-4
benzoic acid 2-hydroxycyclohexyl ester

: 75-36-5
acetyl chloride

: 37844-64-7,64503-98-6,86703-66-4,86703-67-5
(1S,2R)-cis-benzoic acid 2-acetoxycyclohexyl ester

: 188057-87-6
(1R,2S)-cis-benzoic acid 2-hydroxycyclohexyl ester

Guidance literature:: acetyl chloride; With 1,4-diaza-bicyclo[2.2.2]octane; (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; In diethyl ether; at 20 ℃; for 0.0833333h; Inert atmosphere; Resolution of racemate;

benzoic acid 2-hydroxycyclohexyl ester; In diethyl ether; at -20 ℃; for 5h; optical yield given as %ee; Resolution of racemate; Inert atmosphere;
DOI:10.1021/ol301373x

Reference yield:

: 37854-36-7
cis-benzoic acid 2-hydroxycyclohexyl ester

: 108-24-7
acetic anhydride

: 1384068-00-1
(1R,2S)-cis-2-acetoxycyclohexyl benzoate

: 37844-64-7,64503-98-6,86703-66-4,86703-67-5
(1S,2R)-cis-benzoic acid 2-acetoxycyclohexyl ester

: 188057-87-6
(1R,2S)-cis-benzoic acid 2-hydroxycyclohexyl ester

Guidance literature:: With (S)-N-(1-(tert-butylcarbamoyl)-1-(4-(dimethylamino)pyridin-3-yl)methyl)-L-valinemethyl ester; triethylamine; In toluene; at -78 ℃; for 15h; enantioselective reaction;
DOI:10.3987/COM-12-12624