Benzothiazole, 2-(methoxymethyl)- (9CI)

Base Information

• Chemical Name: Benzothiazole, 2-(methoxymethyl)- (9CI)
• CAS No.: 37859-38-4
• Molecular Formula: C9H9NOS
• Molecular Weight: 179.243
• Hs Code.: 2934999090
• Mol file: 37859-38-4.mol

Synonyms:2-methoxymethyl-benzothiazole;2-methoxymethyl-1,3-benzothiazole;2-Methoxymethyl-benzothiazol;2-methoxymethyl-benzonitrile;2-Methoxymethyl-benzonitril;Benzothiazolderivat;

Chemical Property of Benzothiazole, 2-(methoxymethyl)- (9CI)

Chemical Property:

• PSA: 50.36000
• LogP: 2.44270

Purity/Quality:

2-(METHOXYMETHYL)-BENZOTHIAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzothiazole, 2-(methoxymethyl)- (9CI)

There total 2 articles about Benzothiazole, 2-(methoxymethyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloromethylbenzothiazole (37859-43-1) → 2-methoxymethyl-1,3-benzothiazole (37859-38-4) + 2H-1,4-benzothiazin-3-one (5325-20-2) + 2H-3-methoxy-1,4-benzothiazine

Guidance literature:

With sodium methylate; Yield given;

DOI:10.1016/0040-4039(95)00111-O

Reference yield:

2-chloromethylbenzothiazole (37859-43-1) + sodium methylate (124-41-4) → 2-methoxymethyl-1,3-benzothiazole (37859-38-4) + 2H-1,4-benzothiazin-3-one (5325-20-2) + 2H-3-methoxy-1,4-benzothiazine

Guidance literature:

Yield given;

DOI:10.1016/0040-4039(95)00111-O

Reference yield:

2-methoxymethyl-1,3-benzothiazole (37859-38-4) + methyl p-toluene sulfonate (80-48-8) → 2-methoxymethyl-3-methyl-benzothiazolium; toluene-4-sulfonate (37859-44-2)

Guidance literature:

In neat (no solvent); at 140 ℃; for 4h;

DOI:10.1002/hlca.19720550538

upstream raw materials:

2-chloromethylbenzothiazole

sodium methylate

Downstream raw materials:

2-(methoxymethyl)-6-nitrobenzo[d]thiazole

2-methoxymethyl-3-methyl-benzothiazolium; toluene-4-sulfonate

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