Benzaldehyde, 3-chloro-4-(methylthio)-

Base Information

• Chemical Name: Benzaldehyde, 3-chloro-4-(methylthio)-
• CAS No.: 38125-81-4
• Molecular Formula: C8H7ClOS
• Molecular Weight: 186.662
• Mol file: 38125-81-4.mol

Synonyms:3-Chloro-4-methylsulfanyl-benzaldehyde;3-chloro-4-(methylsulfanyl)benzaldehyde;3-Chlor-4-methylmercapto-benzaldehyd;3-chloro-4-methylsulfanylbenzaldehyde;

Chemical Property of Benzaldehyde, 3-chloro-4-(methylthio)-

Chemical Property:

• Melting Point: 58 - 59 °C (ethyl acetate)
• PSA: 42.37000
• LogP: 2.87440

Purity/Quality:

99% ^*data from raw suppliers

3-Chloro-4-methylsulfanyl-benzaldehyde 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzaldehyde, 3-chloro-4-(methylthio)-

There total 4 articles about Benzaldehyde, 3-chloro-4-(methylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

3-Chloro-4-fluorobenzaldehyde (34328-61-5) + sodium thiomethoxide (5188-07-8) → 3-chloro-4-(methylthio)benzaldehyde (38125-81-4)

Guidance literature:

In N,N-dimethyl-formamide; at -10 - 20 ℃;

Reference yield: 30.0%

Dichloromethyl methyl ether (4885-02-3) + 2-chlorothioanisole (17733-22-1) → 3-chloro-4-(methylthio)benzaldehyde (38125-81-4)

Guidance literature:

2-chlorothioanisole; With titanium tetrachloride; In dichloromethane; at -5 - 0 ℃; for 0.333333h;

Dichloromethyl methyl ether; In dichloromethane; at 0 ℃;

Reference yield:

4-methylsulfanyl-3-nitro-benzaldehyde (697306-20-0) → 3-chloro-4-(methylthio)benzaldehyde (38125-81-4)

Guidance literature:

With sodium dithionite; Diazotieren und Umsetzen mit Kupfer(I)-chlorid;

upstream raw materials:

4-methylsulfanyl-3-nitro-benzaldehyde

Dichloromethyl methyl ether

2-chlorothioanisole

3-Chloro-4-fluorobenzaldehyde

Downstream raw materials:

[3-chloro-4-(methylsulfanyl)phenyl](morpholin-4-yl)acetonitrile

4-[4-(3-chloro-4-methylsulfanylphenyl)-3-(diethoxyphosphoryl)-4-hydroxybutyl]piperidine-1-carboxylic acid tert-butyl ester

(3-chloro-4-(methylsulfonyl)phenyl)methanol

4-(bromomethyl)-2-chloro-1-(methylsulfonyl)benzene

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