2,3-Dihydrotetraphen-4(1H)-one

Base Information

Chemical Name:2,3-Dihydrotetraphen-4(1H)-one
CAS No.:38393-90-7
Molecular Formula:C18H14O
Molecular Weight:246.309
Hs Code.:
DSSTox Substance ID:DTXSID60491056
Nikkaji Number:J315.266I
Wikidata:Q82335234
Mol file:38393-90-7.mol

Synonyms:38393-90-7;DTXSID60491056;2,3-Dihydrotetraphen-4(1H)-one;AKOS030255081

Suppliers and Price of 2,3-Dihydrotetraphen-4(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1,2,3,4-Tetrahydrobenz[a]anthracen-4-one
1g
$ 185.00

TRC
1,2,3,4-Tetrahydrobenz[a]anthracen-4-one
500mg
$ 100.00

Total 0 raw suppliers

Chemical Property of 2,3-Dihydrotetraphen-4(1H)-one

Chemical Property:

PSA：17.07000
LogP:4.51200
XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:246.104465066
Heavy Atom Count:19
Complexity:361

Purity/Quality:: 1,2,3,4-Tetrahydrobenz[a]anthracen-4-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=C(C=CC3=CC4=CC=CC=C4C=C23)C(=O)C1
Uses 1,2,3,4-Tetrahydrobenz[a]anthracen-4-one is an intermediate of Benz[a]anthracene-1r,2t,3c,4t-tetrahydro-1,2,3,4-tetrol (B183585), which is an immunosuppressor and a laboratory carcinogen.

Technology Process of 2,3-Dihydrotetraphen-4(1H)-one

There total 1 articles about 2,3-Dihydrotetraphen-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 4483-98-1
1,2,3,4-tetrahydrobenz[a]anthracene

: 56-55-3
benz[a]anthracene

: 38393-90-7
3,4-dihydroxy-benz anthracen-1<2H>-one

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In chloroform; at 65 ℃; for 16h;
DOI:10.1021/jo00153a030

Reference yield:

: 38393-90-7
3,4-dihydroxy-benz anthracen-1<2H>-one

: 316-49-4
4-methylbenz[a]anthracene

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 0 °C

2: p-toluenesulfonic acid / benzene / 0.25 h / 50 °C

3: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 3 h / Heating

With toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In diethyl ether; benzene;
DOI:10.1021/ja00010a036

Reference yield:

: 38393-90-7
3,4-dihydroxy-benz anthracen-1<2H>-one

: 917-54-4
methyllithium

: 316-49-4
4-methylbenz[a]anthracene

Guidance literature:: With tetrahydrofuran; anschliessend Erhitzen in Xylol unter Zusatz von wenig Jod und danach mit Schwefel auf 220-240grad, zuletzt unter Zusatz von Zink-Pulver erhitzen;
DOI:10.1021/jo01100a007