1,2,3,4-Tetrakis(trifluoromethyl)-5-thiabicyclo[2.1.0]pent-2-ene

Base Information

• Chemical Name: 1,2,3,4-Tetrakis(trifluoromethyl)-5-thiabicyclo[2.1.0]pent-2-ene
• CAS No.: 39091-73-1
• Molecular Formula: C8F12S
• Molecular Weight: 356.135
• Mol file: 39091-73-1.mol

Synonyms:5-Thiabicyclo[2.1.0]pent-2-ene,1,2,3,4-tetrakis(trifluoromethyl);perfluorotetramethylDewar-thiophene;tetrakis(trifluoromethyl) Dewar thiophene;1,2,3,4-tetrakis(trifluoromethyl)-5-thiabicyclo{2.1.0}pent-2-ene;

Chemical Property of 1,2,3,4-Tetrakis(trifluoromethyl)-5-thiabicyclo[2.1.0]pent-2-ene

Chemical Property:

• PSA: 25.30000
• LogP: 4.77020

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2,3,4-Tetrakis(trifluoromethyl)-5-thiabicyclo[2.1.0]pent-2-ene

There total 8 articles about 1,2,3,4-Tetrakis(trifluoromethyl)-5-thiabicyclo[2.1.0]pent-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis(trifluoromethyl)thiophene (651-93-4) → 1,2,3,4-tetrakis(trifluoromethyl)-5-thiabicyclo{2.1.0}pent-2-ene (39091-73-1) + hexafluoro-2-butyne (692-50-2)

Guidance literature:

Irradiation (UV/VIS); at 213.9 nm or mercury sensitized 253.7 nm, room temp., 5 Torr;

Reference yield:

hexafluoro-2-butyne (692-50-2) → tetrakis(trifluoromethyl)thiophene (651-93-4) + 1,2,3,4-tetrakis(trifluoromethyl)-5-thiabicyclo{2.1.0}pent-2-ene (39091-73-1) + perfluoro 3,4,5,6-tetramethyl 1,2-dithiin (87721-42-4) + 1a,1b,3,4,4a,5a-Hexakis-trifluoromethyl-1a,1b,4a,5a-tetrahydro-1,2,5-trithia-cyclopropa[a]pentalene (87721-40-2)

Guidance literature:

With carbon oxide sulfide; at 23 ℃; for 0.5h; Yield given. Yields of byproduct given; Irradiation;

Reference yield:

hexafluoro-2-butyne (692-50-2) → tetrakis(trifluoromethyl)thiophene (651-93-4) + 1,2,3,4-tetrakis(trifluoromethyl)-5-thiabicyclo{2.1.0}pent-2-ene (39091-73-1) + 1,2,4,6-Tetrakis-trifluoromethyl-3,5,7-trithia-tricyclo[4.1.0.02,4]heptane (87721-43-5) + 1a,1b,3,4,4a,5a-Hexakis-trifluoromethyl-1a,1b,4a,5a-tetrahydro-1,2,5-trithia-cyclopropa[a]pentalene (87721-40-2)

Guidance literature:

With carbon oxide sulfide; at 23 ℃; for 3.2h; Yield given. Yields of byproduct given; Irradiation;

upstream raw materials:

tetrakis(trifluoromethyl)thiophene

hexafluoro-2-butyne

Downstream raw materials:

8-cyclohexyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.0^2,4]oct-6-ene

tetrakis(trifluoromethyl)thiophene

4-cyclohexyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2.6-diene

C₃₂H₂₆F₁₂N₃P

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