1-Propanol, 3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[4-[2-[[( 1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2-[[[4-[2- [(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]-

Base Information

Chemical Name:1-Propanol, 3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[4-[2-[[( 1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2-[[[4-[2- [(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]-
CAS No.:395069-62-2
Molecular Formula:C62H78O10Si
Molecular Weight:1011.38
Hs Code.:

1-Propanol,
3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[4-[2-[[(
1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2-[[[4-[2-
[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]-

Synonyms:

Suppliers and Price of 1-Propanol, 3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[4-[2-[[( 1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2-[[[4-[2- [(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Propanol, 3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[4-[2-[[( 1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2-[[[4-[2- [(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Propanol, 3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[4-[2-[[( 1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2-[[[4-[2- [(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]-

There total 10 articles about 1-Propanol, 3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[4-[2-[[( 1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2-[[[4-[2- [(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 701911-43-5
[2-(4-bromo-methylphenyl)ethoxy]-tert-butyldiphenylsilane

: 395069-73-5
2-{4-[2-(3,4-dimethoxybenzyloxy)ethyl]benzyloxymethyl}-2-{4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl]benzyloxymethyl}propane-1,3-diol

: 395069-62-2
3-{4-[2-((tert-butyl)diphenylsilyloxy)ethyl]benzyloxy}-2-{4-[2-(3,4-dimethoxybenzyloxy)ethyl]benzyloxymethyl}-2-{4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl]benzyloxymethyl}propan-1-ol

Guidance literature:: 2-{4-[2-(3,4-dimethoxybenzyloxy)ethyl]benzyloxymethyl}-2-{4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl]benzyloxymethyl}propane-1,3-diol; With sodium hydride; In tetrahydrofuran; at 40 ℃; for 0.5h;

[2-(4-bromo-methylphenyl)ethoxy]-tert-butyldiphenylsilane; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; Heating;
DOI:10.1002/ejoc.200600145

Reference yield:

: 13737-36-5
4-bromophenylacetic acid

: 395069-62-2
3-{4-[2-((tert-butyl)diphenylsilyloxy)ethyl]benzyloxy}-2-{4-[2-(3,4-dimethoxybenzyloxy)ethyl]benzyloxymethyl}-2-{4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl]benzyloxymethyl}propan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 86 percent / borane-dimethyl sulfide complex / tetrahydrofuran / 4 h / 0 - 20 °C

2.1: 69 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 20 °C

3.1: NaH / tetrahydrofuran / 0.5 h / 40 °C

3.2: 37 percent / tetrabutylammonium iodide / tetrahydrofuran / Heating

4.1: NaH / tetrahydrofuran / 0.5 h / 40 °C

4.2: 32 percent / tetrabutylammonium iodide / tetrahydrofuran / Heating

With dimethylsulfide borane complex; pyridinium p-toluenesulfonate; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200600145

Reference yield:

: 96044-43-8
4-(2-hydroxyethyl)benzyl bromide

: 395069-62-2
3-{4-[2-((tert-butyl)diphenylsilyloxy)ethyl]benzyloxy}-2-{4-[2-(3,4-dimethoxybenzyloxy)ethyl]benzyloxymethyl}-2-{4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl]benzyloxymethyl}propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 69 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 20 °C

2.1: NaH / tetrahydrofuran / 0.5 h / 40 °C

2.2: 37 percent / tetrabutylammonium iodide / tetrahydrofuran / Heating

3.1: NaH / tetrahydrofuran / 0.5 h / 40 °C

3.2: 32 percent / tetrabutylammonium iodide / tetrahydrofuran / Heating

With pyridinium p-toluenesulfonate; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200600145