4-aMino-1-Methyl-4H-1,2,4-triazol-1-iuM iodide

Base Information

• Chemical Name: 4-aMino-1-Methyl-4H-1,2,4-triazol-1-iuM iodide
• CAS No.: 39602-93-2
• Molecular Formula: C3H7N4.I
• Molecular Weight: 226.02
• Hs Code.: 2933990090
• Mol file: 39602-93-2.mol

Synonyms:Toluene-4-13C;4-amino-1-methyl-1H-1,2,4-triazol-4-ium iodide;4-Amino-1-methyl-1,2,4-triazolium iodide;<4-13C>toluene;Methylbenzene-4-13C;

Chemical Property of 4-aMino-1-Methyl-4H-1,2,4-triazol-1-iuM iodide

Chemical Property:

• Melting Point: 101℃
• PSA: 47.72000
• Density: 1.98 g/cm3
• LogP: -3.99340
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

4-Amino-1-methyl-4H-1,2,4-triazol-1-iumiodide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-aMino-1-Methyl-4H-1,2,4-triazol-1-iuM iodide

There total 1 articles about 4-aMino-1-Methyl-4H-1,2,4-triazol-1-iuM iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-amino-1,2,4-triazole (584-13-4) + methyl iodide (74-88-4) → 4-amino-1-methyl-1H-1,2,4-triazol-4-ium iodide (39602-93-2)

Guidance literature:

In acetonitrile; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1021/jo300611a

Reference yield: 94.0%

sodium 3,6-dinitro-2,5-dihydroxy-1,4-benzoquinone (5357-76-6) + 4-amino-1-methyl-1H-1,2,4-triazol-4-ium iodide (39602-93-2) → 1-methyl-4-amino-1,2,4-triazolium nitranilate

Guidance literature:

In water; at 20 ℃;

DOI:10.1002/chem.200801976

Reference yield: 83.0%

4-amino-1-methyl-1H-1,2,4-triazol-4-ium iodide (39602-93-2) + p-toluenesulfonyl chloride (98-59-9) → N-(1-methyl-1H-1,2,4-triazol-4-ium-4-yl)(tosyl)amide (1382039-29-3)

Guidance literature:

4-amino-1-methyl-1H-1,2,4-triazol-4-ium iodide; p-toluenesulfonyl chloride; With pyridine; at 20 ℃; for 1h; Inert atmosphere;

With sodium hydroxide; In water; Inert atmosphere;

DOI:10.1021/jo300611a

upstream raw materials:

4-amino-1,2,4-triazole

methyl iodide

Downstream raw materials:

1-methyl-4-amino-1,2,4-triazolim perchlorate

1-methyl-4-amino-1,2,4-triazolium nitrate

nitrogen

ammonia

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