3,4-Dimethoxyphenethyl bromide

Base Information

Chemical Name:3,4-Dimethoxyphenethyl bromide
CAS No.:40173-90-8
Molecular Formula:C10H13BrO2
Molecular Weight:245.116
Hs Code.:2909309090
European Community (EC) Number:627-728-7
DSSTox Substance ID:DTXSID70466952
Nikkaji Number:J1.325.767A
Wikidata:Q82293634
Mol file:40173-90-8.mol

Synonyms:3,4-Dimethoxyphenethyl bromide;40173-90-8;4-(2-bromoethyl)-1,2-dimethoxyBenzene;Benzene, 4-(2-bromoethyl)-1,2-dimethoxy-;Homoveratrylbromid;2-Methoxy-4-(2-bromoethyl)anisole;SCHEMBL516206;DTXSID70466952;LTAGXVMHLFYRNK-UHFFFAOYSA-N;4-(bromoethyl)-1,2-dimethoxybenzene;2-(3,4-dimethoxy-phenyl)ethylbromide;2-(3,4-dimethoxyphenyl)-ethylbromide;3,4-Dimethoxyphenethyl bromide, 97%;AKOS012019341;1-(2-bromoethyl)-3,4-dimethoxybenzene;1-bromo-2-(3,4-dimethoxyphenyl)ethane;2-(3,4-dimethoxy-phenyl)-ethylbromide;2-(3,4-dimethoxyphenyl)-ethyl bromide;2-(3,4-dimethoxy-phenyl)-ethyl bromide;1-(2-bromo-ethyl)-3,4-dimethoxy-benzene;CS-0136297;FT-0721840;E85578;EN300-1914292

Suppliers and Price of 3,4-Dimethoxyphenethyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
3,4-Dimethoxyphenethyl bromide 97%
5g
$ 226.00

Sigma-Aldrich
3,4-Dimethoxyphenethyl bromide 97%
1g
$ 49.60

American Custom Chemicals Corporation
3,4-DIMETHOXYPHENETHYL BROMIDE 95.00%
1G
$ 651.49

American Custom Chemicals Corporation
3,4-DIMETHOXYPHENETHYL BROMIDE 95.00%
5G
$ 944.13

AK Scientific
3,4-Dimethoxyphenethyl bromide
1g
$ 236.00

AK Scientific
3,4-Dimethoxyphenethyl bromide
250mg
$ 214.00

AK Scientific
3,4-Dimethoxyphenethyl bromide
100mg
$ 203.00

AK Scientific
3,4-Dimethoxyphenethyl bromide
10g
$ 910.00

Acrotein
3,4-Dimethoxyphenethyl bromide 97%
25g
$ 605.00

Total 13 raw suppliers

Chemical Property of 3,4-Dimethoxyphenethyl bromide

Chemical Property:

Vapor Pressure:0.005mmHg at 25°C
Melting Point:52-56oC(lit.)
Boiling Point:130-131oC3 mm Hg(lit.)
Flash Point:>230 °F
PSA：18.46000
Density:1.336g/cm3
LogP:2.64120
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:244.00989
Heavy Atom Count:13
Complexity:141

Purity/Quality:

99% ^*data from raw suppliers

3,4-Dimethoxyphenethyl bromide 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn,N
Hazard Codes:Xn,N
Statements: 22-36-50
Safety Statements: 26-36/37-61

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)CCBr)OC

Technology Process of 3,4-Dimethoxyphenethyl bromide

There total 5 articles about 3,4-Dimethoxyphenethyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75803-23-5
methanesulphonic acid,2-(3,4-dimethoxyphenyl)ethyl ester

: 40173-90-8
3,4-dimethoxyphenethyl bromide

Guidance literature:: With potassium bromide; In N-methyl-acetamide;

Reference yield:

: 558-13-4
carbon tetrabromide

: 7417-21-2
2-(3,4-dimethoxyphenyl)ethyl alcohol

: 40173-90-8
3,4-dimethoxyphenethyl bromide

Guidance literature:: With triphenylphosphine; In dichloromethane;

Reference yield:

: 5703-21-9
3,4-dimethoxyphenylacetaldehyde

: 40173-90-8
3,4-dimethoxyphenethyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

2: pyridine; phosphorus tribromide / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; phosphorus tribromide; In methanol; dichloromethane;
DOI:10.1021/ol403365