2-(3-Chlorophenyl)-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3-Chlorophenyl)-1,3,2-dioxaborolane
CAS No.:402488-97-5
Molecular Formula:C8H8BClO2
Molecular Weight:182.414
Hs Code.:
DSSTox Substance ID:DTXSID40449196
Nikkaji Number:J1.731.860H
Wikidata:Q82268587
Mol file:402488-97-5.mol

Synonyms:2-(3-chlorophenyl)-1,3,2-dioxaborolane;402488-97-5;1,3,2-Dioxaborolane, 2-(3-chlorophenyl)-;SCHEMBL500331;DTXSID40449196;JOXJSNMBKNEDTQ-UHFFFAOYSA-N;2-(3-chlorophenyl)-[1,3,2]-dioxaborolane

Suppliers and Price of 2-(3-Chlorophenyl)-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-(3-Chlorophenyl)-1,3,2-dioxaborolane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:182.0305874
Heavy Atom Count:12
Complexity:150

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OCCO1)C2=CC(=CC=C2)Cl

Technology Process of 2-(3-Chlorophenyl)-1,3,2-dioxaborolane

There total 1 articles about 2-(3-Chlorophenyl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 108-37-2
1-bromo-3-chlorobenzene

: 107-21-1
ethylene glycol

: 402488-97-5
3-chlorophenylboronic acid ethylene glycol ester

Guidance literature:: 1-bromo-3-chlorobenzene; With magnesium; In tetrahydrofuran;

With Trimethyl borate; In tetrahydrofuran; at -78 - 20 ℃;

ethylene glycol; In toluene; Further stages.; Heating;
DOI:10.1021/jo011073j

Reference yield: 81.0%

: 402488-97-5
3-chlorophenylboronic acid ethylene glycol ester

: 2050-67-1
PCB 11

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium diacetate; tetraethylammonium perchlorate; potassium carbonate; In water; acetonitrile; at 20 ℃; Inert atmosphere; Electrochemical reaction;
DOI:10.1016/j.tet.2009.08.004

Reference yield: 77.0%

: 695-12-5,25498-06-0
vinylcyclohexane

: 402488-97-5
3-chlorophenylboronic acid ethylene glycol ester

: (E)-1-chloro-3-(2-cyclohexylvinyl)benzene

Guidance literature:: With oxygen; palladium diacetate; copper(II) bis(trifluoromethanesulfonate); In N,N-dimethyl acetamide; at 40 ℃; for 48h; regioselective reaction;
DOI:10.1021/acs.orglett.0c00061