7-Oxabicyclo[2.2.1]hepta-2,5-diene-2,3-dicarboxylic acid, 1-[[(3-methyl-2-butenyl)[(4-methylphenyl)sulfonyl]amino]methyl]-, dimethyl ester

Base Information

Chemical Name:7-Oxabicyclo[2.2.1]hepta-2,5-diene-2,3-dicarboxylic acid, 1-[[(3-methyl-2-butenyl)[(4-methylphenyl)sulfonyl]amino]methyl]-, dimethyl ester
CAS No.:403790-45-4
Molecular Formula:C23H27NO7S
Molecular Weight:461.536
Hs Code.:
Mol file:403790-45-4.mol

7-Oxabicyclo[2.2.1]hepta-2,5-diene-2,3-dicarboxylic acid,
1-[[(3-methyl-2-butenyl)[(4-methylphenyl)sulfonyl]amino]methyl]-,
dimethyl ester

Synonyms:

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Chemical Property of 7-Oxabicyclo[2.2.1]hepta-2,5-diene-2,3-dicarboxylic acid, 1-[[(3-methyl-2-butenyl)[(4-methylphenyl)sulfonyl]amino]methyl]-, dimethyl ester

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Technology Process of 7-Oxabicyclo[2.2.1]hepta-2,5-diene-2,3-dicarboxylic acid, 1-[[(3-methyl-2-butenyl)[(4-methylphenyl)sulfonyl]amino]methyl]-, dimethyl ester

There total 4 articles about 7-Oxabicyclo[2.2.1]hepta-2,5-diene-2,3-dicarboxylic acid, 1-[[(3-methyl-2-butenyl)[(4-methylphenyl)sulfonyl]amino]methyl]-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 762-42-5
dimethyl acetylenedicarboxylate

: 403790-44-3
N-(3-methylbut-2-enyl)-N-(4-tolylsulfonyl)-2-furfurylamine

: 403790-45-4
1-{[(3-methyl-but-2-enyl)-(toluene-4-sulfonyl)-amino]-methyl}-7-oxa-bicyclo[2.2.1]hepta-2,5-diene-2,3-dicarboxylic acid dimethyl ester

Guidance literature:: With hydroquinone; In dichloromethane; at 20 ℃; for 528h;
DOI:10.1039/b204778k

Reference yield:

: 617-89-0
furan-2-ylmethanamine

: 403790-45-4
1-{[(3-methyl-but-2-enyl)-(toluene-4-sulfonyl)-amino]-methyl}-7-oxa-bicyclo[2.2.1]hepta-2,5-diene-2,3-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / pyridine / 4 h / 0 °C

2.1: NaH / dimethylformamide / 1 h / 20 °C

2.2: 50 percent / dimethylformamide / 20 h / 20 °C

3.1: 54 percent / hydroquinone / CH₂Cl₂ / 528 h / 20 °C

With pyridine; sodium hydride; hydroquinone; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b204778k

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 403790-45-4
1-{[(3-methyl-but-2-enyl)-(toluene-4-sulfonyl)-amino]-methyl}-7-oxa-bicyclo[2.2.1]hepta-2,5-diene-2,3-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / pyridine / 4 h / 0 °C

2.1: NaH / dimethylformamide / 1 h / 20 °C

2.2: 50 percent / dimethylformamide / 20 h / 20 °C

3.1: 54 percent / hydroquinone / CH₂Cl₂ / 528 h / 20 °C

With pyridine; sodium hydride; hydroquinone; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b204778k