Bis(4-nitrophenyl)phosphoric Acid Sodium Salt

Base Information

• Chemical Name: Bis(4-nitrophenyl)phosphoric Acid Sodium Salt
• CAS No.: 4043-96-3
• Molecular Formula: C12H9N2O8P.Na
• Molecular Weight: 362.168
• Hs Code.: 2919900090
• Mol file: 4043-96-3.mol

Synonyms:Bis(4-nitrophenyl)phosphoric Acid Sodium Salt;Bis(4-nitrophenyl) hydrogen phosphate (sodium);Bis(p-nitrophenyl) phosphate sodium salt, >=99% (TLC)

Chemical Property of Bis(4-nitrophenyl)phosphoric Acid Sodium Salt

Chemical Property:

• Vapor Pressure: 9.64E-13mmHg at 25°C
• Boiling Point: 545.7oC at 760 mmHg
• Flash Point: 283.8oC
• PSA: 160.04000
• LogP: 4.54580
• Storage Temp.: −20°C
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 4
• Exact Mass: 362.99942153
• Heavy Atom Count: 24
• Complexity: 434

Purity/Quality:

97% ^*data from raw suppliers

Sodium Bis(4-nitrophenyl) Phosphate [for Phosphodiesterase Substrate] >98.0%(HPLC)(T) ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC(=CC=C1[N+](=O)[O-])OP(=O)(O)OC2=CC=C(C=C2)[N+](=O)[O-].[Na]
• Uses: Bis(p-nitrophenyl) phosphate sodium salt has been used as a substrate for the estimation of phosphodiesterase (PDE) activity. It has also been used as a substrate in PDE inhibition assay.

Technology Process of Bis(4-nitrophenyl)phosphoric Acid Sodium Salt

There total 1 articles about Bis(4-nitrophenyl)phosphoric Acid Sodium Salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C12H8N2O8P(1-)*C30H57N6(3+)*2Cl(1-) → C30H57N6(3+)*3Cl(1-) + sodium bis(4-nitrophenyl) phosphate (4043-96-3)

Guidance literature:

With sodium chloride; In d⁽⁴⁾-methanol; at 65 ℃; Equilibrium constant;

DOI:10.1002/ejoc.200901516

Reference yield: 92.0%

zinc perchlorate + [Fe(CH2(CH2NHCHC6H2(O)(CH3)CHNCH2)2CH2)(OH2)Cl](2+)*2ClO4(1-)*2H2O=C24H30Cl3FeN4O11*2H2O + sodium bis(4-nitrophenyl) phosphate (4043-96-3) → [(Fe((C6H2(O)(CH3)CHN(CH2)3NCH)2)Zn(μ-bis(4-nitrophenyl)phosphato))2(μ-O)](ClO4)2

Guidance literature:

With (C₂H₅)3N; In methanol; acetonitrile; Zn salt and a MeOH soln. of ligand salt added to a MeCN soln. of Fe complex; crystd. overnight, filtered, recrystd. (MeOH/MeCN); elem. anal.;

DOI:10.1021/ic060183b

Reference yield: 90.0%

nickel(II) perchlorate hexahydrate + ((CH3C6H2OH(CHN)2)2(CH2)6)Fe(H2O)Cl(2+)*2ClO4(1-)*2H2O=((CH3C6H2OH(CHN)2)2(CH2)6)Fe(H2O)Cl(ClO4)2*2H2O + sodium bis(4-nitrophenyl) phosphate (4043-96-3) → [(bis(4-nitrophenyl)phosphate)Fe((CH2C6H2O(CHN)2)2(CH2)6)(μ-bis(4-nitrophenyl)phosphate)Ni(H2O)]ClO4

Guidance literature:

In water; acetonitrile; CH3CN coln. of Fe complex treated with solid Ni salt (1 equiv.) and 5 equiv. of bis(4-nitrophenyl)phosphate, reacted for 1 h; filtered, washed (H2O, EtOH), recrystd.(CH3CN/CH3OH 1:1), elem. anal.;

DOI:10.1016/j.poly.2011.09.009

Downstream raw materials:

4-nitro-phenol

sodium p-nitrophenyl hydrogen phosphate

mono-p-nitrophenyl phosphate

dimethylphosphoric acid

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