[2-(Cyclohex-2-en-1-yl)ethyl]benzene

Base Information

Chemical Name:[2-(Cyclohex-2-en-1-yl)ethyl]benzene
CAS No.:40463-34-1
Molecular Formula:C14H18
Molecular Weight:186.297
Hs Code.:
DSSTox Substance ID:DTXSID90513174
Nikkaji Number:J2.018.702F
Mol file:40463-34-1.mol

Synonyms:40463-34-1;[2-(Cyclohex-2-en-1-yl)ethyl]benzene;DTXSID90513174

Suppliers and Price of [2-(Cyclohex-2-en-1-yl)ethyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of [2-(Cyclohex-2-en-1-yl)ethyl]benzene

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:186.140850574
Heavy Atom Count:14
Complexity:175

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC=CC(C1)CCC2=CC=CC=C2

Technology Process of [2-(Cyclohex-2-en-1-yl)ethyl]benzene

There total 8 articles about [2-(Cyclohex-2-en-1-yl)ethyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 103-63-9
1-phenyl-2-bromoethane

: 1521-51-3,113667-32-6
rac-3-bromocyclohexene

: 40463-34-1
(2-(cyclohex-2-en-1-yl)ethyl)benzene

Guidance literature:: 1-phenyl-2-bromoethane; With magnesium; In tetrahydrofuran; at 20 ℃; for 0.5h;

rac-3-bromocyclohexene; In tetrahydrofuran; for 8h; Further stages.;
DOI:10.1055/s-2008-1072561

Reference yield: 70.0%

: 17376-04-4
2-phenethyl iodide

: 1521-51-3,113667-32-6
rac-3-bromocyclohexene

: 40463-34-1
(2-(cyclohex-2-en-1-yl)ethyl)benzene

Guidance literature:: With palladium diacetate; copper(II) acetate monohydrate; ammonium bromide; lithium chloride; In water; N,N-dimethyl-formamide; at 0 ℃; for 12h; Electrochemical reaction;
DOI:10.1021/acs.orglett.7b00473

Reference yield:

: 76644-52-5,76704-31-9,14447-34-8,62247-41-0
rac-3-acetoxycyclohexene

: 29443-41-2
β-phenylethylidenehydrazine

: 40463-34-1
(2-(cyclohex-2-en-1-yl)ethyl)benzene

Guidance literature:: rac-3-acetoxycyclohexene; With bis(η3-allyl-μ-chloropalladium(II)); Tri(p-tolyl)phosphine; In tetrahydrofuran; for 0.5h; Schlenk technique; Sealed tube; Inert atmosphere;

β-phenylethylidenehydrazine; With lithium tert-butoxide; In tetrahydrofuran; at 45 ℃; for 24h; chemoselective reaction; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1002/anie.201809112