Isoquinoline, 5,8-dibromo-1,2-dihydro-6,7-dimethoxy-2-[(2R)-2-[[(4-nitrophenyl)sulfon yl]amino]-1-oxopropyl]-1-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl]-, (1S)-

Base Information

Chemical Name:Isoquinoline, 5,8-dibromo-1,2-dihydro-6,7-dimethoxy-2-[(2R)-2-[[(4-nitrophenyl)sulfon yl]amino]-1-oxopropyl]-1-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl]-, (1S)-
CAS No.:405555-09-1
Molecular Formula:C31H31Br2N3O11S
Molecular Weight:813.475
Hs Code.:
Mol file:405555-09-1.mol

Isoquinoline,
5,8-dibromo-1,2-dihydro-6,7-dimethoxy-2-[(2R)-2-[[(4-nitrophenyl)sulfon
yl]amino]-1-oxopropyl]-1-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl]-, (1S)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Isoquinoline, 5,8-dibromo-1,2-dihydro-6,7-dimethoxy-2-[(2R)-2-[[(4-nitrophenyl)sulfon yl]amino]-1-oxopropyl]-1-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl]-, (1S)-

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Isoquinoline, 5,8-dibromo-1,2-dihydro-6,7-dimethoxy-2-[(2R)-2-[[(4-nitrophenyl)sulfon yl]amino]-1-oxopropyl]-1-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl]-, (1S)-

There total 2 articles about Isoquinoline, 5,8-dibromo-1,2-dihydro-6,7-dimethoxy-2-[(2R)-2-[[(4-nitrophenyl)sulfon yl]amino]-1-oxopropyl]-1-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl]-, (1S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852852-86-9
2-(R)-(4-nitrophenylsulfonamido)propanoic acid

: 405555-09-1
5,8-dibromo-1,2-dihydro-6,7-dimethoxy-2-[N-(4-nitrobenzenesulfonyl)-(R)-alanyl]-1-(S)-(3,4,5-trimethoxyphenacyl)isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: SOCl₂ / benzene / 8 h / 60 °C

2.1: CH₂Cl₂ / -78 °C

2.2: CH₂Cl₂ / 1 h / -78 °C

With thionyl chloride; In dichloromethane; benzene;
DOI:10.1248/cpb.51.951