Methanol, [methylenebis(oxy)]bis-, diacetate

Base Information

• Chemical Name: Methanol, [methylenebis(oxy)]bis-, diacetate
• CAS No.: 4082-92-2
• Molecular Formula: C7H12O6
• Molecular Weight: 192.169
• Mol file: 4082-92-2.mol

Synonyms:

Chemical Property of Methanol, [methylenebis(oxy)]bis-, diacetate

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methanol, [methylenebis(oxy)]bis-, diacetate

There total 8 articles about Methanol, [methylenebis(oxy)]bis-, diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-Trioxan (110-88-3) + acetic anhydride (108-24-7) → diacetoxymethane (628-51-3,25231-38-3) + bis(acetoxymethyl)ether (4082-91-1,25231-38-3) + bis-acetoxymethoxy-methane (4082-92-2,25231-38-3)

Guidance literature:

With perchloric acid; at -60 ℃; for 1.16667h;

DOI:10.1039/c8cy01691g

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + bis(acetoxymethyl)ether (4082-91-1,25231-38-3) → diacetoxymethane (628-51-3,25231-38-3) + bis-acetoxymethoxy-methane (4082-92-2,25231-38-3) + 1,7-diacetoxy-2,4,6-trioxa-heptane (27969-30-8,25231-38-3)

Guidance literature:

at 140 - 150 ℃;

Reference yield:

→ bis-acetoxymethoxy-methane (4082-92-2,25231-38-3)

Guidance literature:

With hydrogenchloride; at 180 ℃; Fraktionieren im HCl-Strom und Behandeln der bei 160-170grad destillierenden Fraktion mit geschmolzenem Natriumacetat;

upstream raw materials:

formaldehyd

diacetoxymethane

bis(acetoxymethyl)ether

acetic anhydride

Downstream raw materials:

bis<(2,4,6-trichlorophenoxy)methyl> ether

Refernces