Vanadium, tetrakis(phenylmethyl)-

Base Information

Chemical Name:Vanadium, tetrakis(phenylmethyl)-
CAS No.:41328-40-9
Molecular Formula:C28H28V
Molecular Weight:415.472
Hs Code.:

Synonyms:

Suppliers and Price of Vanadium, tetrakis(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Vanadium, tetrakis(phenylmethyl)-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Vanadium, tetrakis(phenylmethyl)-

There total 2 articles about Vanadium, tetrakis(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131063-11-1,16997-51-6,19559-06-9
Vanadium (III) chloride-(tris-tetrahydrofuran)

: 6921-34-2
benzylmagnesium chloride

: 25377-37-1,27790-75-6,82009-22-1
Tetrakis(pyridin)-dichlorovanadin(II)

: 41328-40-9
tetrabenzylvanadium

: 7786-30-3
magnesium chloride

Guidance literature:: In diethyl ether; 1 mol of complex was slowly added to an ether soln. of 2 mol RMgCl at -15°C, after 1 h the temp. was raised to 0°C (Ar atm.);; dioxane in hexane was added, ppt. was filtered off, identified by ESR spectra;;
DOI:10.1016/S0022-328X(00)82672-8

Reference yield:

: 41328-40-9
tetrabenzylvanadium

Guidance literature:: VCl4, Mg(CH2Ph)2;
DOI:10.1016/S0022-328X(00)94150-0

Reference yield: 50.0%

: 41328-40-9
tetrabenzylvanadium

: 78628-04-3
dibenzylvanadium-bis(2-benzylpropyl-2-oxide)

Guidance literature:: With acetone; In diethyl ether; Ar, acetone added to a soln. of V-compound in a ratio of 4:1 at -20°C, temp. raised to 20°C; solvent removed under reduced pressure, extd. (pentane), pentane removed in vacuo;
DOI:10.1007/BF01558080