1-Methyl-1H-iMidazole-5-carbonyl chloride

Base Information

Chemical Name:1-Methyl-1H-iMidazole-5-carbonyl chloride
CAS No.:41716-12-5
Molecular Formula:C5H5ClN2O
Molecular Weight:144.56
Hs Code.:2933290090
Mol file:41716-12-5.mol

Synonyms:1-methyl-1H-imidazole-5-carboxylic acid chloride;1-Methyl-5-imidazoliecarboxylic hydrazide;1-Methyl-5-imidazolcarbonsaeurechlorid;3-Methyl-3H-imidazol-4-carbonsaeure-hydrazid;1-Methyl-imidazol-5-carbohydrazid;3-methyl-3H-imidazole-4-carboxylic acid hydrazide;1-methyl-1H-imidazole-5-carboxylic acid hydrazide;1-Methyl-5-carboxyhydrazid-imidazol;1-Methyl-imidazol-5-carbonsaeurechlorid;3-methyl-3H-imidazole-4-carbonyl chloride;1-Methyl-1H-imidazole-5-carbohydrazide;

Suppliers and Price of 1-Methyl-1H-iMidazole-5-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-METHYL-1H-IMIDAZOLE-5-CARBONYL CHLORIDE 95.00%
5MG
$ 503.00

Total 3 raw suppliers

Chemical Property of 1-Methyl-1H-iMidazole-5-carbonyl chloride

Chemical Property:

Boiling Point:296.7±13.0 °C(Predicted)
PKA:3.02±0.10(Predicted)
PSA：34.89000
Density:1.37±0.1 g/cm3(Predicted)
LogP:0.79910

Purity/Quality:

99% ^*data from raw suppliers

1-METHYL-1H-IMIDAZOLE-5-CARBONYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Methyl-1H-iMidazole-5-carbonyl chloride

There total 3 articles about 1-Methyl-1H-iMidazole-5-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 41806-40-0
1-methyl-1H-imidazole-5-carboxylic acid

: 41716-12-5
3-methyl-3H-imidazole-4-carbonyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; for 1h; Heating / reflux;

Reference yield:

: 19485-38-2
1-methyl-1H-imidazole-4,5-dicarboxylic acid

: 41716-12-5
3-methyl-3H-imidazole-4-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Ac₂O / 4 h / 100 °C / selectivity of decarboxylation; other acid anhydride; var. temp. reaction time and solvents

2: SOCl₂ / 6 h / Heating

With thionyl chloride; acetic anhydride;
DOI:10.1246/bcsj.53.557