methyl dotriacontanoate

Base Information

• Chemical Name: methyl dotriacontanoate
• CAS No.: 41755-79-7
• Molecular Formula: C33H66O2
• Mol file: 41755-79-7.mol

Synonyms:

Chemical Property of methyl dotriacontanoate

Chemical Property:

• Vapor Pressure: 7.77E-10mmHg at 25°C

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl dotriacontanoate

There total 8 articles about methyl dotriacontanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1α,3β,30-trihydroxy-29-carboxy-olean-9(11),12-diene-3-dotriacontanoate → dotriacontanoic acid methyl ester (41755-79-7)

Guidance literature:

With potassium hydroxide; In methanol; at 20 ℃; for 0.25h;

DOI:10.7717/peerj.13040

Reference yield:

8-[2-(5-Docosyl-thiophen-2-yl)-[1,3]dithiolan-2-yl]-octanoic acid methyl ester (111515-00-5) → dotriacontanoic acid methyl ester (41755-79-7)

Guidance literature:

With W₆ Raney nickel; In ethanol; Heating;

Reference yield:

methyl 9-chloro-9-oxononanoate (56555-02-3) → dotriacontanoic acid methyl ester (41755-79-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 60 percent / stannic chloride / benzene / 2 h / Ambient temperature

2: BF₃(OC₂H₅)3 / CHCl₃ / Ambient temperature

3: W₆ Raney nickel / ethanol / Heating

With BF₃(OC₂H₅)3; W₆ Raney nickel; tin(IV) chloride; In ethanol; chloroform; benzene;

upstream raw materials:

methanol

8-[2-(5-Docosyl-thiophen-2-yl)-[1,3]dithiolan-2-yl]-octanoic acid methyl ester

methyl 9-chloro-9-oxononanoate

2-Behenyl-thiophene

Refernces

• 1、 Al-Hamoud, Gadah A.,Al-Musayeib, Nawal M.,Amina, Musarat,Ibrahim, Sabrin R. M.. "Abubidentin A, New Oleanane-type Triterpene Ester from Abutilon bidentatum and its antioxidant, cholinesterase and antimicrobial activities". . . Retrieved 2022/03/18.
• 2、 Kuwahara, Yasumasa. "Lacceryl laccerate: Major Wax Component Produced by Anomoneura mori Schwarz (Homoptera: Psyllidae)". . p. 1297 - 1300. Retrieved 2007/10/02.