9-Methyl-9-butyl-9H-fluorene

Base Information

Chemical Name:9-Methyl-9-butyl-9H-fluorene
CAS No.:42348-92-5
Molecular Formula:C18H20
Molecular Weight:
Hs Code.:
Mol file:42348-92-5.mol

Synonyms:

Suppliers and Price of 9-Methyl-9-butyl-9H-fluorene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-Methyl-9-butyl-9H-fluorene

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 9-Methyl-9-butyl-9H-fluorene

There total 3 articles about 9-Methyl-9-butyl-9H-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 542-69-8
1-iodo-butane

: 2523-37-7
9-methylfluorene

: 42348-92-5
9-methyl-9-butylfluorene

Guidance literature:: 9-methylfluorene; With n-butyllithium; tert-butylisonitrile; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 - 20 ℃;

1-iodo-butane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at 0 ℃; for 0.5h; Further stages.;
DOI:10.1021/jo0001479

Reference yield:

: 109-65-9
1-bromo-butane

: 31468-21-0
9-methylfluorenyl carboanion

: 42348-92-5
9-methyl-9-butylfluorene

Guidance literature:: In dimethyl sulfoxide; at 25 ℃; Thermodynamic data; ΔG⁰;
DOI:10.1021/jo00281a035

Reference yield:

: 109-65-9
1-bromo-butane

: 38024-80-5
cesium salt of 9-methylfluorene

: 42348-92-5
9-methyl-9-butylfluorene

Guidance literature:: In 1,2-dimethoxyethane; at 25 ℃; Rate constant; The rate constants for the free carbanions and the ion pairs were calculated;