1-Methyl-1-propylcyclohexane.

Base Information

• Chemical Name: 1-Methyl-1-propylcyclohexane.
• CAS No.: 4258-93-9
• Molecular Formula: C10H20
• Molecular Weight: 140.269
• Hs Code.: 2902199090
• Mol file: 4258-93-9.mol

Synonyms:Cyclohexane, 1-methyl-1-propyl-;1-Methyl-1-propyl-cyclohexan;Cyclohexane,1-methyl-1-propyl;1-methyl-1-propyl-cyclohexane;

Chemical Property of 1-Methyl-1-propylcyclohexane.

Chemical Property:

• Vapor Pressure: 2.06mmHg at 25°C
• Melting Point: -84.33°C (estimate)
• Refractive Index: 1.4440
• Boiling Point: 169.3oC at 760 mmHg
• Flash Point: 45.2oC
• PSA: 0.00000
• Density: 0.783g/cm3
• LogP: 3.75690

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Methyl-1-propylcyclohexane.

There total 14 articles about 1-Methyl-1-propylcyclohexane. which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

tetrapropylsilane (994-66-1) + 1-chloro-1-methylcyclohexane (931-78-2) → 3-propyl, 1-methylcyclohexane (4291-80-9) + 1-methyl-1-propylcyclohexane (4258-93-9) + 1-methyl-2-propyl-cyclohexane (4291-79-6,4926-71-0,42806-77-9,130365-42-3,130365-43-4,130365-46-7,130365-47-8,130365-50-3,130365-51-4) + methyl cyclohexane (82166-21-0)

Guidance literature:

With aluminium trichloride; In dichloromethane; for 1h; Product distribution; Ambient temperature; various ratios, various time, various Lewis acids;

Reference yield: 4.0%

tetramethylsilane (75-76-3) + 1-propylcyclohexene (2539-75-5) → propylcyclohexane (1678-92-8) + 1-methyl-1-propylcyclohexane (4258-93-9)

Guidance literature:

With hydrogenchloride; aluminium trichloride; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

propyl-cycloheptane (13705-36-7) → 1-methyl-1-propylcyclohexane (4258-93-9) + phenylpropane (103-65-1)

Guidance literature:

at 320 ℃;

DOI:10.1016/S0953-7562(08)61976-0

upstream raw materials:

1-chloro-1-methylcyclohexane

n-propylmagnesium bromide

di-n-propyl zinc

1-(1-methyl-cyclohexyl)-propan-1-one

Downstream raw materials:

phenylpropane

toluene

Refernces

• 1、 Bolestova, G. I.,Parnes, Z. N.. "IONIC ALKYLATION OF TERTIARY ALKYL HALIDES WITH TETRAALKYLSILANES". . p. 32 - 36. Retrieved 2007/10/02.