2,8-dibromophenoxathiine

Base Information

Chemical Name:2,8-dibromophenoxathiine
CAS No.:56348-81-3
Molecular Formula:C12H6Br2OS
Molecular Weight:358.0484
Hs Code.:

Synonyms:

Suppliers and Price of 2,8-dibromophenoxathiine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2,8-dibromophenoxathiine

Chemical Property:

Vapor Pressure:2.34E-06mmHg at 25°C
Boiling Point:403.6°C at 760 mmHg
Flash Point:197.9°C
Density:1.894g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,8-dibromophenoxathiine

There total 3 articles about 2,8-dibromophenoxathiine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 262-20-4
phenoxathiine

: 56348-81-3
2,8-dibromo-phenoxathiine

Guidance literature:: With hydrogen bromide; bromine; at 0 - 20 ℃; for 12.5h; Inert atmosphere;

Reference yield:

: 56348-81-3
2,8-dibromo-phenoxathiine

Guidance literature:: With copper(II) sulfate; at 150 ℃;
DOI:10.1039/jr9310000718

Reference yield:

: 101-84-8
diphenylether

: 56348-81-3
2,8-dibromo-phenoxathiine

Guidance literature:: Multi-step reaction with 2 steps

1: sulfur; aluminum (III) chloride / dichloromethane / 4 h / 70 - 100 °C

2: hydrogen bromide; bromine / 12.5 h / 0 - 20 °C / Inert atmosphere

With aluminum (III) chloride; hydrogen bromide; bromine; sulfur; In dichloromethane;