Technology Process of Phenol, 2-amino-5-(methylsulfonyl)-
There total 6 articles about Phenol, 2-amino-5-(methylsulfonyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen; acetic acid;
In
tetrahydrofuran; ethanol;
at 20 ℃;
for 18h;
DOI:10.1021/jm500610n
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / dichloromethane / 18 h / 0 - 20 °C
2: tetrahydrofuran; water / 72 h / 20 °C
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18 h / 20 °C
4: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethanol / 18 h / 20 °C
5: palladium 10% on activated carbon; hydrogen; acetic acid / tetrahydrofuran; ethanol / 18 h / 20 °C
With
pyridine; palladium 10% on activated carbon; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm500610n
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrahydrofuran; water / 72 h / 20 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18 h / 20 °C
3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethanol / 18 h / 20 °C
4: palladium 10% on activated carbon; hydrogen; acetic acid / tetrahydrofuran; ethanol / 18 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm500610n
