Carbamic acid, [4-hydroxy-1-(4-hydroxyphenyl)butyl]methyl-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [4-hydroxy-1-(4-hydroxyphenyl)butyl]methyl-, 1,1-dimethylethyl ester
CAS No.:444646-45-1
Molecular Formula:C16H25NO4
Molecular Weight:295.379
Hs Code.:

Synonyms:

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Chemical Property of Carbamic acid, [4-hydroxy-1-(4-hydroxyphenyl)butyl]methyl-, 1,1-dimethylethyl ester

Chemical Property:

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Technology Process of Carbamic acid, [4-hydroxy-1-(4-hydroxyphenyl)butyl]methyl-, 1,1-dimethylethyl ester

There total 12 articles about Carbamic acid, [4-hydroxy-1-(4-hydroxyphenyl)butyl]methyl-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 444646-44-0
N-[1-(4-benzyloxyphenyl)-4-hydroxybutyl]-N-methylcarbamic acid tert-butyl ester

: 444646-45-1
t-butyl N-[4-hydroxybutyl-1-(4-hydroxyphenyl)]-N-methylcarbamate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 4h;

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 444646-45-1
t-butyl N-[4-hydroxybutyl-1-(4-hydroxyphenyl)]-N-methylcarbamate

Guidance literature:: Multi-step reaction with 12 steps

1.1: ethanol / 2 h / 90 °C

2.1: sulfuric acid / 6 h / 80 °C

3.1: tetrahydrofuran / 12 h / 20 °C

4.1: K₂CO₃ / dimethylformamide / 3 h / 20 °C

5.1: LiAlH₄ / tetrahydrofuran / 0.17 h / -20 - -10 °C

6.1: 2.20 g / NaOH / H₂O; methanol / 2 h / 50 °C

7.1: 1.90 g / K₂CO₃ / acetone / 2 h / 50 °C

8.1: 2.24 g / Et₃N / tetrahydrofuran / 1 h / 20 °C

9.1: 1.54 g / 15-crown-5 / dimethylformamide / 12 h / 20 °C

10.1: diisobutylaluminium hydride / CH₂Cl₂; hexane / 2 h / -78 - 20 °C

10.2: NH₄Cl / H₂O

11.1: 351 mg / NaBH₄ / methanol / 0.33 h / 20 °C

12.1: 274 mg / H₂ / 5 percent Pd/C / methanol / 4 h / 20 °C

With sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; 15-crown-5; sulfuric acid; hydrogen; diisobutylaluminium hydride; potassium carbonate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 10303-89-6
3-(4-hydroxy-phenyl)-3-methylamino-propionic acid

: 444646-45-1
t-butyl N-[4-hydroxybutyl-1-(4-hydroxyphenyl)]-N-methylcarbamate

Guidance literature:: Multi-step reaction with 11 steps

1.1: sulfuric acid / 6 h / 80 °C

2.1: tetrahydrofuran / 12 h / 20 °C

3.1: K₂CO₃ / dimethylformamide / 3 h / 20 °C

4.1: LiAlH₄ / tetrahydrofuran / 0.17 h / -20 - -10 °C

5.1: 2.20 g / NaOH / H₂O; methanol / 2 h / 50 °C

6.1: 1.90 g / K₂CO₃ / acetone / 2 h / 50 °C

7.1: 2.24 g / Et₃N / tetrahydrofuran / 1 h / 20 °C

8.1: 1.54 g / 15-crown-5 / dimethylformamide / 12 h / 20 °C

9.1: diisobutylaluminium hydride / CH₂Cl₂; hexane / 2 h / -78 - 20 °C

9.2: NH₄Cl / H₂O

10.1: 351 mg / NaBH₄ / methanol / 0.33 h / 20 °C

11.1: 274 mg / H₂ / 5 percent Pd/C / methanol / 4 h / 20 °C

With sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; 15-crown-5; sulfuric acid; hydrogen; diisobutylaluminium hydride; potassium carbonate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone;