Chloroacetic acid, hexyl ester

Base Information

• Chemical Name: Chloroacetic acid, hexyl ester
• CAS No.: 5927-57-1
• Molecular Formula: C8H15 Cl O2
• Molecular Weight: 178.659
• Mol file: 5927-57-1.mol

Synonyms:Aceticacid, chloro-, hexyl ester (7CI,8CI,9CI); Chloroacetic acid hexyl ester; Hexylchloroacetate; NSC 22576; n-Hexyl chloroacetate

Chemical Property of Chloroacetic acid, hexyl ester

Chemical Property:

• Vapor Pressure: 0.166mmHg at 25°C
• Boiling Point: 213.2°C at 760 mmHg
• Flash Point: 102.3°C
• PSA: 26.30000
• Density: 1.018g/cm³
• LogP: 2.34870

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Chloroacetic acid, hexyl ester

There total 3 articles about Chloroacetic acid, hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

chloroacetyl chloride (79-04-9) + hexan-1-ol (111-27-3) → chloroacetic acid n-hexylester (5927-57-1)

Guidance literature:

In dichloromethane; at 30 - 40 ℃; Large scale;

Reference yield: 64.0%

chloroacetic acid (79-11-8) + hexan-1-ol (111-27-3) → chloroacetic acid n-hexylester (5927-57-1)

Guidance literature:

With p-toluenesulfonic acid monohydrate; In toluene;

DOI:10.1134/S1070363217050085

Reference yield:

→ chloroacetic acid n-hexylester (5927-57-1)

Guidance literature:

Chloressigsaeure, Hexan-1-ol ;

upstream raw materials:

chloroacetyl chloride

hexan-1-ol

chloroacetic acid

Downstream raw materials:

(4-oxo-2-phenyl-4H-chromen-7-yloxy)-acetic acid hexyl ester

Hexyloxycarbonylmethyl-triphenyl-phosphonium-chlorid

Refernces

• 1、 Zhuravlev,Voronchikhina. "Synthesis and physico-chemical properties of ionic liquids—3-methyl-1-alkyloxycarbonylmethylpyridinium hexafluorophosphates". . p. 940 - 944. Retrieved 2017/06/28.
• 2、 Jobe, David J.,Reinsborough, Vincent C.. "Micellar properties of sodium alkyl sulfoacetates and sodium dialkyl sulfosuccinates in water". . p. 280 - 284. Retrieved 2007/10/02.