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Chloroacetyl Chloride
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79-04-9 Usage

79-04-9 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (C0098)  Chloroacetyl Chloride  >98.0%(GC)(T) 79-04-9 25g 180.00CNY Detail
TCI America (C0098)  Chloroacetyl Chloride  >98.0%(GC)(T) 79-04-9 100g 290.00CNY Detail
TCI America (C0098)  Chloroacetyl Chloride  >98.0%(GC)(T) 79-04-9 500g 480.00CNY Detail
Alfa Aesar (A15846)  Chloroacetyl chloride, 98%    79-04-9 25ml 111.0CNY Detail
Alfa Aesar (A15846)  Chloroacetyl chloride, 98%    79-04-9 250ml 528.0CNY Detail
Alfa Aesar (A15846)  Chloroacetyl chloride, 98%    79-04-9 500ml 949.0CNY Detail
Alfa Aesar (A15846)  Chloroacetyl chloride, 98%    79-04-9 2500ml 1100.0CNY Detail

79-04-9SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Chloroacetyl chloride

1.2 Other means of identification

Product number -
Other names CHLOROACETYL CHLORIDE FOR PHARMA SYNTHESIS

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Intermediates,Ion exchange agents
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:79-04-9 SDS

79-04-9Synthetic route

2-chloro-3,3-dimethyl-1-butene
27843-27-2

2-chloro-3,3-dimethyl-1-butene

A

tert-butyl phosphinyl dichloride
4707-95-3

tert-butyl phosphinyl dichloride

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

C

phosphoryl chloride

phosphoryl chloride

Conditions
ConditionsYield
With oxygen; phosphorus trichloride at -10 - 10℃;A 90%
B n/a
C n/a
With oxygen; phosphorus trichloride at -10 - 10℃; Product distribution; Mechanism;A 90%
B n/a
C n/a
acetyl chloride
75-36-5

acetyl chloride

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With chlorine at 55℃; under 750.075 - 1500.15 Torr; Temperature;89.59%
With chlorine im Sonnenlicht;
With iodine durch Chlorieren;
With tetrachloromethane; chlorine Irradiation.im Licht der Quarzlampe;
chloroacetic acid
79-11-8

chloroacetic acid

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With thionyl chloride In N,N-dimethyl-formamide at 20℃; for 24h;70%
With phosphorus trichloride
With thionyl chloride
cis/trans-3,5-Bis-(chloromethyl)-3-fluoro-5-methyl-1,2,4-trioxolane
173063-66-6

cis/trans-3,5-Bis-(chloromethyl)-3-fluoro-5-methyl-1,2,4-trioxolane

A

chloroacetone
78-95-5

chloroacetone

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

C

Chloro-acetic acid 1,2-dichloro-1-methyl-ethyl ester

Chloro-acetic acid 1,2-dichloro-1-methyl-ethyl ester

Conditions
ConditionsYield
With triphenylphosphine In chloroform-d1A 28 % Spectr.
B 23 % Spectr.
C 33%
Ketene
463-51-4

Ketene

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With nitrosylchloride
With chlorine in der Gasphase;
With tetrachloromethane; chlorine
With sulfur dioxide; chlorine
With diethyl ether; chlorine
Ketene
463-51-4

Ketene

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With chlorine in der Gasphase;
Ketene
463-51-4

Ketene

A

nitroacetyl chloride
6061-03-6

nitroacetyl chloride

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With diethyl ether; Nitryl chloride Kuehlung mit CO2-Alkohol;
1,2-Dichloroethylene
540-59-0

1,2-Dichloroethylene

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With sulfuric acid; oxygen
With bromine; oxygen
1,1-Dichloroethylene
75-35-4

1,1-Dichloroethylene

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With tetrachloromethane; oxygen; chlorine Irradiation.unter UV-Bestrahlung;
With oxygen; chlorine Irradiation.unter UV-Bestrahlung , ohne Loesungsmittel;
With oxygen; chlorine; chloroacetyl chloride Irradiation.unter UV-Bestrahlung;
(E)-1,2-dichloro-1-ethoxy-ethene
42345-82-4

(E)-1,2-dichloro-1-ethoxy-ethene

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With hydrogenchloride und nachtraegliches Erhitzen;
With hydrogenchloride
1,1-dichloroethyl chloroacetate
13398-09-9

1,1-dichloroethyl chloroacetate

A

2-chloroethanal
107-20-0

2-chloroethanal

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
Spaltung;
Benzotrichlorid
98-07-7

Benzotrichlorid

(E)-3-Ureido-but-2-enoic acid ethyl ester
5435-44-9, 22243-66-9

(E)-3-Ureido-but-2-enoic acid ethyl ester

chloroacetic acid
79-11-8

chloroacetic acid

A

benzoyl chloride
98-88-4

benzoyl chloride

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
at 80 - 90℃;
Benzotrichlorid
98-07-7

Benzotrichlorid

chloroacetic acid
79-11-8

chloroacetic acid

A

benzoyl chloride
98-88-4

benzoyl chloride

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
at 100 - 120℃;
Benzotrichlorid
98-07-7

Benzotrichlorid

chloroacetic acid
79-11-8

chloroacetic acid

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
at 100 - 120℃;
With zinc(II) chloride at 80 - 90℃;
phosgene
75-44-5

phosgene

chloroacetic acid
79-11-8

chloroacetic acid

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With pyrographite at 200℃;
With anionenexchanger at 150℃;
oxalyl dichloride
79-37-8

oxalyl dichloride

chloroacetic acid
79-11-8

chloroacetic acid

chloroacetyl chloride
79-04-9

chloroacetyl chloride

oxalyl dichloride
79-37-8

oxalyl dichloride

Chloroacetic anhydride
541-88-8

Chloroacetic anhydride

chloroacetyl chloride
79-04-9

chloroacetyl chloride

dimethylsulfide
75-18-3

dimethylsulfide

3,5-Dichloro-3,5-bis-chloromethyl-[1,2,4]trioxolane

3,5-Dichloro-3,5-bis-chloromethyl-[1,2,4]trioxolane

A

2-chloroethanal
107-20-0

2-chloroethanal

B

chloro-methylsulfanyl-methane
2373-51-5

chloro-methylsulfanyl-methane

C

chloroacetic acid
79-11-8

chloroacetic acid

D

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
In chloroform-d1 Ambient temperature;A 10 % Spectr.
B 35 % Spectr.
C 31 % Spectr.
D 25 % Spectr.
acetyl chloride
75-36-5

acetyl chloride

chloroacetic acid
79-11-8

chloroacetic acid

A

acetic acid
64-19-7

acetic acid

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
In various solvent(s) at 39.9℃; Equilibrium constant; Kinetics; Thermodynamic data; var. temp.; activation energy E;
(dichloroacetyl)methylphenylphosphane
102099-45-6

(dichloroacetyl)methylphenylphosphane

A

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

C

methyl(phenyl)chlorophosphine
15849-86-2, 540513-01-7

methyl(phenyl)chlorophosphine

Conditions
ConditionsYield
at 0 - 35℃; for 4h; Mechanism; var. time, with solv.; other chloroacetylphosphanes;
3-Chlor-3,5-bis(chlormethyl)-1,2,4-trioxolan
173063-63-3

3-Chlor-3,5-bis(chlormethyl)-1,2,4-trioxolan

A

chloroacetic acid
79-11-8

chloroacetic acid

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
In chloroform-d1 at 41℃; for 312h;A 61 % Spectr.
B 38 % Spectr.
cis/trans-3,5-Bis-(chloromethyl)-3-fluoro-5-methyl-1,2,4-trioxolane
173063-66-6

cis/trans-3,5-Bis-(chloromethyl)-3-fluoro-5-methyl-1,2,4-trioxolane

A

dichloro-acetic acid
79-43-6

dichloro-acetic acid

B

acetyl chloride
75-36-5

acetyl chloride

C

chloroacetyl chloride
79-04-9

chloroacetyl chloride

D

5-Chlor-2-(chlormethyl)-2-methyl-1,3-dioxolan-4-on

5-Chlor-2-(chlormethyl)-2-methyl-1,3-dioxolan-4-on

Conditions
ConditionsYield
With 1,1,2,2-tetrachloroethane In chloroform-d1 at 23℃; for 240h;A 15 % Spectr.
B 25 % Spectr.
C 8 % Spectr.
D 9 % Spectr.
(Chloracetyl)(1,2-dichlor-1-methylethyl)peroxid
153940-11-5

(Chloracetyl)(1,2-dichlor-1-methylethyl)peroxid

A

chloroacetone
78-95-5

chloroacetone

B

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With triphenylphosphine In chloroform-d1 Ambient temperature;A 54 % Spectr.
B 42 % Spectr.
3,5-Dichloro-3,5-bis-chloromethyl-[1,2,4]trioxolane

3,5-Dichloro-3,5-bis-chloromethyl-[1,2,4]trioxolane

A

2-chloroethanal
107-20-0

2-chloroethanal

B

chloro-methylsulfanyl-methane
2373-51-5

chloro-methylsulfanyl-methane

C

chloroacetic acid
79-11-8

chloroacetic acid

D

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With dimethylsulfide In chloroform-d1 Ambient temperature;A 10 % Spectr.
B 35 % Spectr.
C 31 % Spectr.
D 25 % Spectr.
3,5-Dichloro-3,5-bis-chloromethyl-[1,2,4]trioxolane

3,5-Dichloro-3,5-bis-chloromethyl-[1,2,4]trioxolane

A

dichloro-acetic acid
79-43-6

dichloro-acetic acid

B

dichloroacethyl chloride
79-36-7

dichloroacethyl chloride

C

chloroacetic acid
79-11-8

chloroacetic acid

D

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
In chloroform-d1 at 60℃; for 168h;A 9 % Spectr.
B 8 % Spectr.
C 22 % Spectr.
D 60 % Spectr.
acetic acid
64-19-7

acetic acid

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With hydrogenchloride; N-chloro-succinimide; thionyl chloride; acetic acid 1.) 70 deg C, 30 min, 2.) 85 deg C, 90 min; Yield given. Multistep reaction;
1,2-dichloro-ethane
107-06-2

1,2-dichloro-ethane

A

formyl chloride
2565-30-2

formyl chloride

B

carbon dioxide
124-38-9

carbon dioxide

C

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With oxygen; chlorine In gas at 22.9℃; under 700 Torr; Rate constant; Irradiation; pulse radiolysis;
trans-1,2-dichloroethylene
156-60-5

trans-1,2-dichloroethylene

A

formic acid
64-18-6

formic acid

B

formyl chloride
2565-30-2

formyl chloride

C

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With water; oxygen for 0.0152778h; Quantum yield; Decomposition; UV-irradiation;
chloroethylene
75-01-4

chloroethylene

A

2-chloroethanal
107-20-0

2-chloroethanal

B

formyl chloride
2565-30-2

formyl chloride

C

chloroacetyl chloride
79-04-9

chloroacetyl chloride

D

acetylene
74-86-2

acetylene

Conditions
ConditionsYield
With oxygen for 0.0152778h; Quantum yield; Decomposition; UV-irradiation;
1,1-Dichloroethylene
75-35-4

1,1-Dichloroethylene

A

formic acid
64-18-6

formic acid

B

formyl chloride
2565-30-2

formyl chloride

C

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
With water; oxygen for 0.00833333h; Quantum yield; Decomposition; UV-irradiation;
pyrrolidine
123-75-1

pyrrolidine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

chloroacetic acid pyrrolidide
20266-00-6

chloroacetic acid pyrrolidide

Conditions
ConditionsYield
In acetone at 20℃;100%
In tetrahydrofuran at 0 - 20℃; for 3.5h;99%
In tetrahydrofuran at 20℃; for 12h; Acylation;98%
piperidine
110-89-4

piperidine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

1-chloroacetyl-piperidine
1440-60-4

1-chloroacetyl-piperidine

Conditions
ConditionsYield
In acetone at 20℃;100%
With triethylamine In dichloromethane at 0 - 10℃; for 1h;100%
With triethylamine In dichloromethane at 0 - 20℃; for 6h;98%
morpholine
110-91-8

morpholine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

N-chloroacetylmorpholine
1440-61-5

N-chloroacetylmorpholine

Conditions
ConditionsYield
With potassium carbonate In toluene at 60℃; for 2h;100%
Stage #1: morpholine; chloroacetyl chloride With triethylamine In dichloromethane at 0 - 27℃; for 2h;
Stage #2: With hydrogenchloride In dichloromethane; water
100%
With triethylamine In dichloromethane at 0 - 20℃; for 6h;99%
TETRAHYDROFURFURYLAMINE
4795-29-3

TETRAHYDROFURFURYLAMINE

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-[(tetrahydrofuran-2-yl)methyl]acetamide
39089-62-8

2-chloro-N-[(tetrahydrofuran-2-yl)methyl]acetamide

Conditions
ConditionsYield
In dichloromethane100%
With potassium carbonate In dichloromethane Heating;97%
With trimethylamine In dichloromethane at 0 - 20℃; for 4h;76%
1-indoline
496-15-1

1-indoline

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-Chloro-1-(2,3-dihydro-1H-1-indolyl)-1-ethanone
17133-48-1

2-Chloro-1-(2,3-dihydro-1H-1-indolyl)-1-ethanone

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 3h;100%
With N,N-dimethyl acetamide at 0℃; for 0.0833333h; Green chemistry;89%
In acetone at 0 - 20℃; for 1h;63%
tryptamine
61-54-1

tryptamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-<2-(indol-3-yl)ethyl>acetamide
52191-26-1

2-chloro-N-<2-(indol-3-yl)ethyl>acetamide

Conditions
ConditionsYield
With potassium carbonate In dichloromethane Ambient temperature;100%
In dichloromethane100%
With triethylamine In tetrahydrofuran at 20℃; for 6h; Cooling with ice; Inert atmosphere;96%
isobutylamine
78-81-9

isobutylamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-isobutylacetamide
32461-83-9

2-chloro-N-isobutylacetamide

Conditions
ConditionsYield
In acetone at 20℃;100%
With potassium carbonate In dichloromethane at 20℃; Cooling with ice;73%
With potassium carbonate In dichloromethane at 20℃; Cooling with ice;73.1%
2,4-Dichloroaniline
554-00-7

2,4-Dichloroaniline

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-(2,4-dichlorophenyl)acetamide
6974-56-7

2-chloro-N-(2,4-dichlorophenyl)acetamide

Conditions
ConditionsYield
Stage #1: 2,4-Dichloroaniline With triethylamine In dichloromethane at 20℃; for 0.5h;
Stage #2: chloroacetyl chloride In dichloromethane at 0℃;
100%
With triethylamine In dichloromethane at 0 - 25℃;99.4%
With triethylamine In dichloromethane at 0 - 25℃;99.4%
cyclohexylamine
108-91-8

cyclohexylamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-Chloro-N-cyclohexylacetamide
23605-23-4

2-Chloro-N-cyclohexylacetamide

Conditions
ConditionsYield
In dichloromethane100%
With triethylamine In dichloromethane at 20 - 27℃; for 1h;100%
In acetonitrile at 5 - 20℃; for 2h;93%
4-methoxy-aniline
104-94-9

4-methoxy-aniline

chloroacetyl chloride
79-04-9

chloroacetyl chloride

N-(4-methoxyphenyl)-2-chloroacetamide
22303-36-2

N-(4-methoxyphenyl)-2-chloroacetamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 0℃; for 0.166667h;100%
In tetrahydrofuran at 20℃; for 18h;100%
With triethylamine In dichloromethane at 0 - 25℃;99.4%
2-(3,4-dimethoxyphenyl)-ethylamine
120-20-7

2-(3,4-dimethoxyphenyl)-ethylamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-(2-(3,4-dimethoxyphenyl)ethyl)acetamide
14301-31-6

2-chloro-N-(2-(3,4-dimethoxyphenyl)ethyl)acetamide

Conditions
ConditionsYield
In dichloromethane100%
With N,N-dimethyl-aniline In dichloromethane at 0℃; for 1h;98%
With N,N-dimethyl-aniline In dichloromethane at 0℃; for 2h;98%
phenethylamine
64-04-0

phenethylamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-phenethylacetamide
13156-95-1

2-chloro-N-phenethylacetamide

Conditions
ConditionsYield
With potassium carbonate In dichloromethane Ambient temperature;100%
With potassium carbonate In dichloromethane at 20℃; Acylation;100%
In dichloromethane100%
diphenylamine
122-39-4

diphenylamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N,N-diphenylacetamide
5428-43-3

2-chloro-N,N-diphenylacetamide

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 0.333333h;100%
In toluene at 90℃; for 4h; Inert atmosphere;99%
In N,N-dimethyl-formamide at 80℃; for 2h;97%
diethylamine
109-89-7

diethylamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-Chloro-N,N-diethylacetamide
2315-36-8

2-Chloro-N,N-diethylacetamide

Conditions
ConditionsYield
In dichloromethane; water at 5℃; Temperature; Solvent;100%
With triethylamine In dichloromethane at 0℃;99%
With triethylamine In 1,2-dichloro-ethane at 10 - 20℃; for 3h; Cooling with ice;95%
2-Aminobenzyl alcohol
5344-90-1

2-Aminobenzyl alcohol

chloroacetyl chloride
79-04-9

chloroacetyl chloride

[2-(2-chloro-acetylamino)-phenyl]-methanol
189940-09-8

[2-(2-chloro-acetylamino)-phenyl]-methanol

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h;100%
With diethyl ether; benzene
With triethylamine In tetrahydrofuran75.9 g (93%)
With triethylamine In tetrahydrofuran75.9 g (93%)
With triethylamine In tetrahydrofuran75.9 g (93%)
propylamine
107-10-8

propylamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

N-(propyl)chloroacetamide
13916-39-7

N-(propyl)chloroacetamide

Conditions
ConditionsYield
In dichloromethane100%
In dichloromethane at 0℃; for 1h; Inert atmosphere;100%
In dichloromethane for 1h; Cooling with ice; Inert atmosphere;99%
2-amino-1-phenylpropane
60-15-1, 156-34-3, 51-64-9, 300-62-9

2-amino-1-phenylpropane

chloroacetyl chloride
79-04-9

chloroacetyl chloride

(+/-)-chloroacetic acid-(1-methyl-2-phenyl-ethylamide)
13156-94-0

(+/-)-chloroacetic acid-(1-methyl-2-phenyl-ethylamide)

Conditions
ConditionsYield
With potassium carbonate In dichloromethane Ambient temperature;100%
(-)-menthol
2216-51-5

(-)-menthol

chloroacetyl chloride
79-04-9

chloroacetyl chloride

Conditions
ConditionsYield
In benzene Heating;100%
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 12h; Temperature;98.8%
With pyridine In dichloromethane at 0 - 20℃; for 1.33333h; Inert atmosphere;98%
chloroacetyl chloride
79-04-9

chloroacetyl chloride

aniline
62-53-3

aniline

N-chloroacetyl-aniline
587-65-5

N-chloroacetyl-aniline

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere;100%
With potassium carbonate In acetone at 20℃; for 4h;98%
With triethylamine In dichloromethane at 15℃; for 0.25h;98.55%
chloroacetyl chloride
79-04-9

chloroacetyl chloride

3-chloro-aniline
108-42-9

3-chloro-aniline

2-chloro-N-(3-chlorophenyl)acetamide
2564-05-8

2-chloro-N-(3-chlorophenyl)acetamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 25℃;100%
With triethylamine In dichloromethane at 0 - 25℃;100%
In tetrahydrofuran at 20℃; for 18h;100%
chloroacetyl chloride
79-04-9

chloroacetyl chloride

3,5-Dichloroaniline
626-43-7

3,5-Dichloroaniline

2-chloro-N-(3,5-dichlorophenyl)acetamide
33560-48-4

2-chloro-N-(3,5-dichlorophenyl)acetamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 25℃;100%
With triethylamine In dichloromethane at 0 - 25℃;100%
With triethylamine In dichloromethane at 20℃; for 5h;99%
chloroacetyl chloride
79-04-9

chloroacetyl chloride

benzylamine
100-46-9

benzylamine

N-benzyl-2-chloroacetamide
2564-06-9

N-benzyl-2-chloroacetamide

Conditions
ConditionsYield
In dichloromethane100%
With triethylamine In dichloromethane at 0 - 20℃; for 4h; Inert atmosphere;98%
With potassium carbonate In dichloromethane Heating;97%
chloroacetyl chloride
79-04-9

chloroacetyl chloride

4-fluoroaniline
371-40-4

4-fluoroaniline

2-chloro-N-(4-fluorophenyl)acetamide
351-04-2

2-chloro-N-(4-fluorophenyl)acetamide

Conditions
ConditionsYield
In ethyl acetate for 3h; Heating;100%
With potassium hydrogencarbonate In Isopropyl acetate; water at 0 - 20℃; for 0.5h;95%
With triethylamine In dichloromethane at 0 - 20℃; for 5h; Inert atmosphere;95%
chloroacetyl chloride
79-04-9

chloroacetyl chloride

1-acetyl-2-phenylhydrazine
114-83-0

1-acetyl-2-phenylhydrazine

2-acetyl-1-(2-chloroacetyl)phenylhydrazine
108511-46-2

2-acetyl-1-(2-chloroacetyl)phenylhydrazine

Conditions
ConditionsYield
In dichloromethane for 0.5h;100%
With benzene
chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-(3-methoxyphenyl)-1-ethanamine
2039-67-0

2-(3-methoxyphenyl)-1-ethanamine

N-chloroacetyl-N-(2-(3-methoxy-phenyl)-ethyl)-amine
34162-12-4

N-chloroacetyl-N-(2-(3-methoxy-phenyl)-ethyl)-amine

Conditions
ConditionsYield
With potassium carbonate In dichloromethane Ambient temperature;100%
With sodium hydrogencarbonate In dichloromethane at 0 - 20℃; for 2h;93%
With triethylamine In dichloromethane at 0 - 20℃; for 2h;73%
chloroacetyl chloride
79-04-9

chloroacetyl chloride

Phentermin
122-09-8

Phentermin

2-chloro-N-(2-methyl-1-phenylpropan-2-yl)acetamide
26187-18-8

2-chloro-N-(2-methyl-1-phenylpropan-2-yl)acetamide

Conditions
ConditionsYield
With potassium carbonate In dichloromethane Ambient temperature;100%
6-methylbenzothiazol-2-ylamine
2536-91-6

6-methylbenzothiazol-2-ylamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-(6-methylbenzothiazol-2-yl)acetamide
3174-15-0

2-chloro-N-(6-methylbenzothiazol-2-yl)acetamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃;100%
Stage #1: 6-methylbenzothiazol-2-ylamine With pyridine In benzene at 0 - 5℃; for 0.5h;
Stage #2: chloroacetyl chloride In benzene for 2h;
92%
With triethylamine In chloroform at 20℃; for 2h;91%
4-(4-chlorophenyl)-2-thiazolamine
2103-99-3

4-(4-chlorophenyl)-2-thiazolamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-[4-(4-chlorophenyl)-1,3-thiazol-2-yl]acetamide
6125-31-1

2-chloro-N-[4-(4-chlorophenyl)-1,3-thiazol-2-yl]acetamide

Conditions
ConditionsYield
Stage #1: 4-(4-chlorophenyl)-2-thiazolamine With triethylamine In dichloromethane at 0 - 5℃; for 0.5h;
Stage #2: chloroacetyl chloride In dichloromethane at 0 - 20℃; for 2h;
100%
With pyridine for 6.5h;81%
In benzene for 3h; Reflux;65%
[2-(2-thyenyl)ethyl]amine
30433-91-1

[2-(2-thyenyl)ethyl]amine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-(2-(thiophen-2-yl)ethyl)acetamide
135709-69-2

2-chloro-N-(2-(thiophen-2-yl)ethyl)acetamide

Conditions
ConditionsYield
With potassium carbonate In dichloromethane Ambient temperature;100%
With triethylamine In dichloromethane at 0℃;82%
In benzene at 0℃; Reflux;
2-(3-thienyl)ethylamine
59311-67-0

2-(3-thienyl)ethylamine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-(2-(thiophen-3-yl)ethyl)acetamide
135709-70-5

2-chloro-N-(2-(thiophen-3-yl)ethyl)acetamide

Conditions
ConditionsYield
With potassium carbonate In dichloromethane Ambient temperature;100%
With triethylamine In dichloromethane at 0℃;2.2 g
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