Piperazine, 1-methyl-4-[(3-nitrophenyl)sulfonyl]-

Base Information

Chemical Name:Piperazine, 1-methyl-4-[(3-nitrophenyl)sulfonyl]-
CAS No.:453562-01-1
Molecular Formula:C11H15N3O4S
Molecular Weight:285.324
Hs Code.:

Synonyms:3-[(4-methylpiperazinyl)sulfonyl]-1-nitrobenzene;1-Methyl-4-[(3-nitrophenyl)sulfonyl]piperazine;

Suppliers and Price of Piperazine, 1-methyl-4-[(3-nitrophenyl)sulfonyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Piperazine, 1-methyl-4-[(3-nitrophenyl)sulfonyl]-

Chemical Property:

PSA：94.82000
LogP:2.01070

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Piperazine, 1-methyl-4-[(3-nitrophenyl)sulfonyl]-

There total 5 articles about Piperazine, 1-methyl-4-[(3-nitrophenyl)sulfonyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.37%

: 109-01-3
1-methyl-piperazine

: 121-51-7
3-nitrobenzenesulphonyl chloride

: 453562-01-1
3-[(4-methylpiperazinyl)-sulfonyl]-1-nitrobenzene

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 5h;

Reference yield:

: 109-01-3
1-methyl-piperazine

: 97-08-5
3-nitro-4-chlorosulfonyl chloride

: 453562-01-1
3-[(4-methylpiperazinyl)-sulfonyl]-1-nitrobenzene

Guidance literature:: With triethylamine; In dichloromethane; at -40 ℃; for 1h;

Reference yield:

: 127-68-4
sodium 3-nitrobenzenesulfonate

: 453562-01-1
3-[(4-methylpiperazinyl)-sulfonyl]-1-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate; N,N-dimethyl-formamide / acetonitrile / 2 h / 72 - 75 °C

2: triethylamine / dichloromethane / 5 h / 20 °C

With triethylamine; N,N-dimethyl-formamide; trichlorophosphate; In dichloromethane; acetonitrile;