BIS(1H,1H,2H,2H,3H,3H-PERFLUORONONYL) AZODICARBOXYLATE

Base Information

Chemical Name:BIS(1H,1H,2H,2H,3H,3H-PERFLUORONONYL) AZODICARBOXYLATE
CAS No.:462996-01-6
Molecular Formula:C20H12F26N2O4
Molecular Weight:838.27900
Hs Code.:
Mol file:462996-01-6.mol

Synonyms:Bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl) azodicarboxylate;4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl (NE)-N-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononoxycarbonylimino)carbamate;

Suppliers and Price of BIS(1H,1H,2H,2H,3H,3H-PERFLUORONONYL) AZODICARBOXYLATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
Bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl) azodicarboxylate ≥90%
5g-f
$ 777.00

Sigma-Aldrich
Bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl) azodicarboxylate ≥90%
1g-f
$ 182.00

American Custom Chemicals Corporation
BIS(4,4,5,5,6,6,7,7,8,8,9,9,9-TRIDECAFLUORONONYL) AZODICARBOXYLATE 95.00%
5G
$ 1577.79

American Custom Chemicals Corporation
BIS(4,4,5,5,6,6,7,7,8,8,9,9,9-TRIDECAFLUORONONYL) AZODICARBOXYLATE 95.00%
1G
$ 807.69

Total 3 raw suppliers

Chemical Property of BIS(1H,1H,2H,2H,3H,3H-PERFLUORONONYL) AZODICARBOXYLATE

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:56-60oC
Boiling Point:410.666oC at 760 mmHg
Flash Point:202.164oC
PSA：77.32000
Density:1.644g/cm3
LogP:10.74980
Storage Temp.:−20°C

Purity/Quality:

97% ^*data from raw suppliers

Bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl) azodicarboxylate ≥90% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of BIS(1H,1H,2H,2H,3H,3H-PERFLUORONONYL) AZODICARBOXYLATE

There total 3 articles about BIS(1H,1H,2H,2H,3H,3H-PERFLUORONONYL) AZODICARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 462995-97-7
1,2-bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl)hydrazine dicarboxylate

: 462996-01-6
bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl) diazodicarboxylate

Guidance literature:: With pyridine; bromine; In dichloromethane; at 20 ℃;
DOI:10.1016/S0040-4020(02)00205-3

Reference yield:

: 80806-68-4
4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononan-1-ol

: 462996-01-6
bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl) diazodicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 20 °C

2: hydrazine monochloride; triethylamine / tetrahydrofuran / 20 °C

3: pyridine; bromine / CH₂Cl₂ / 20 °C

With pyridine; hydrazine hydrochloride; bromine; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(02)00205-3

Reference yield:

: imidazole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl ester

: 462996-01-6
bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl) diazodicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine monochloride; triethylamine / tetrahydrofuran / 20 °C

2: pyridine; bromine / CH₂Cl₂ / 20 °C

With pyridine; hydrazine hydrochloride; bromine; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(02)00205-3