Technology Process of Benzamide, N-[2-[(aminoiminomethyl)amino]ethyl]-
There total 5 articles about Benzamide, N-[2-[(aminoiminomethyl)amino]ethyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 740 mg / H2 / 10percent Pd/C / ethanol / 24 h / 3102.9 Torr
2: 73 percent / ethanol / 48 h / Heating
3: 720 mg / anhydrous ammonia, triethylamine, silver nitrate / acetonitrile / 12 h
4: liquid NH3, Na, NH4Cl
With
ammonia; hydrogen; sodium; ammonium chloride; silver nitrate; triethylamine;
palladium on activated charcoal;
In
ethanol; acetonitrile;
DOI:10.1021/jo00325a006
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 88 percent / triethylamine / diethyl ether
2: 740 mg / H2 / 10percent Pd/C / ethanol / 24 h / 3102.9 Torr
3: 73 percent / ethanol / 48 h / Heating
4: 720 mg / anhydrous ammonia, triethylamine, silver nitrate / acetonitrile / 12 h
5: liquid NH3, Na, NH4Cl
With
ammonia; hydrogen; sodium; ammonium chloride; silver nitrate; triethylamine;
palladium on activated charcoal;
In
diethyl ether; ethanol; acetonitrile;
DOI:10.1021/jo00325a006
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 73 percent / ethanol / 48 h / Heating
2: 720 mg / anhydrous ammonia, triethylamine, silver nitrate / acetonitrile / 12 h
3: liquid NH3, Na, NH4Cl
With
ammonia; sodium; ammonium chloride; silver nitrate; triethylamine;
In
ethanol; acetonitrile;
DOI:10.1021/jo00325a006
