2-Oxa-4,6,11-triazadodec-4-en-12-oic acid, 10-(carboxymethyl)-6-methyl-3-oxo-1-phenyl-5-[[(phenylmethoxy)carbon yl]amino]-, 12-(phenylmethyl) ester, (10S)-

Base Information

Chemical Name:2-Oxa-4,6,11-triazadodec-4-en-12-oic acid, 10-(carboxymethyl)-6-methyl-3-oxo-1-phenyl-5-[[(phenylmethoxy)carbon yl]amino]-, 12-(phenylmethyl) ester, (10S)-
CAS No.:468071-25-2
Molecular Formula:C32H36N4O8
Molecular Weight:604.66
Hs Code.:

2-Oxa-4,6,11-triazadodec-4-en-12-oic acid,
10-(carboxymethyl)-6-methyl-3-oxo-1-phenyl-5-[[(phenylmethoxy)carbon
yl]amino]-, 12-(phenylmethyl) ester, (10S)-

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Chemical Property of 2-Oxa-4,6,11-triazadodec-4-en-12-oic acid, 10-(carboxymethyl)-6-methyl-3-oxo-1-phenyl-5-[[(phenylmethoxy)carbon yl]amino]-, 12-(phenylmethyl) ester, (10S)-

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Technology Process of 2-Oxa-4,6,11-triazadodec-4-en-12-oic acid, 10-(carboxymethyl)-6-methyl-3-oxo-1-phenyl-5-[[(phenylmethoxy)carbon yl]amino]-, 12-(phenylmethyl) ester, (10S)-

There total 3 articles about 2-Oxa-4,6,11-triazadodec-4-en-12-oic acid, 10-(carboxymethyl)-6-methyl-3-oxo-1-phenyl-5-[[(phenylmethoxy)carbon yl]amino]-, 12-(phenylmethyl) ester, (10S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 468071-23-0
N^β,N^ω,N^ω'-tris(benzyloxycarbonyl)-N^ε-methyl-(S)-β-homoarginine tert-butyl ester

: 468071-25-2
N^β,N^ω,N^ω'-tris(benzyloxycarbonyl)-N^ε-methyl-(S)-β-homoarginine

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at -5 ℃;
DOI:10.1021/jm0111191

Reference yield:

: 152120-55-3
N,N-bis(benzyloxycarbonyl)-1H-pyrazole-1-carboxamidine

: 468071-25-2
N^β,N^ω,N^ω'-tris(benzyloxycarbonyl)-N^ε-methyl-(S)-β-homoarginine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Et₃N / CH₂Cl₂ / Heating

2: 59 percent / Et₃SiH; TFA / CH₂Cl₂ / -5 °C

With triethylsilane; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm0111191

Reference yield:

: N^β-benzyloxycarbonyl-N^ε-methyl-(S)-β-lysine tert-butyl ester hydrochloride

: 468071-25-2
N^β,N^ω,N^ω'-tris(benzyloxycarbonyl)-N^ε-methyl-(S)-β-homoarginine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Et₃N / CH₂Cl₂ / Heating

2: 59 percent / Et₃SiH; TFA / CH₂Cl₂ / -5 °C

With triethylsilane; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm0111191