Nonanedioic acid, monobutyl ester

Base Information

• Chemical Name: Nonanedioic acid, monobutyl ester
• CAS No.: 4753-32-6
• Molecular Formula: C13H24O4
• Molecular Weight: 244.331
• Mol file: 4753-32-6.mol

Synonyms:

Chemical Property of Nonanedioic acid, monobutyl ester

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Nonanedioic acid, monobutyl ester

There total 1 articles about Nonanedioic acid, monobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-butane (109-65-9) + azelaic acid (123-99-9,26776-28-3) → di-butyl azelate (2917-73-9) + Nonanedioic acid monobutyl ester (4753-32-6)

Guidance literature:

With sodium hydroxide; Aliquat 336; In toluene; for 24h; Heating;

DOI:10.1016/0040-4020(89)80151-6

Reference yield:

Nonanedioic acid monobutyl ester (4753-32-6) → 8-[5,7-Dimethoxy-3-(4-methoxy-phenyl)-4-oxo-4H-chromen-2-yl]-octanoic acid butyl ester

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / oxalyl chloride / 2 h / Heating

2: 84 percent / pyridine / 48 h / Ambient temperature

3: 68 percent / Et₃N, TMSCl / dimethylformamide / 48 h / Heating

With pyridine; chloro-trimethyl-silane; oxalyl dichloride; triethylamine; In N,N-dimethyl-formamide;

DOI:10.1055/s-1998-2221

Reference yield:

Nonanedioic acid monobutyl ester (4753-32-6) → Nonanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester (218899-26-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / oxalyl chloride / 2 h / Heating

2: 84 percent / pyridine / 48 h / Ambient temperature

With pyridine; oxalyl dichloride;

DOI:10.1055/s-1998-2221

upstream raw materials:

1-bromo-butane

azelaic acid

Downstream raw materials:

Nonanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester