5-HYDROXY-2-PHENYL-BENZOFURAN-3-CARBOXYLIC ACID ETHYL ESTER

Base Information

Chemical Name:5-HYDROXY-2-PHENYL-BENZOFURAN-3-CARBOXYLIC ACID ETHYL ESTER
CAS No.:4610-75-7
Molecular Formula:C17H14O4
Molecular Weight:282.296
Hs Code.:
Mol file:4610-75-7.mol

Synonyms:ethyl 5-hydroxy-2-phenylbenzofuran-3-carboxylate;3-ethoxycarbonyl-5-hydroxy-2-phenyl-1-benzofuran;5-Hydroxy-2-phenyl-benzofuran-3-carboxylic acid ethyl ester;2-Phenyl-3-carbaethoxy-5-hydroxybenzofuran;2-Phenyl-3-ethoxycarbonyl-5-hydroxybenzofuran;5-Hydroxy-2-phenyl-benzofuran-3-carbonsaeure-aethylester;

Suppliers and Price of 5-HYDROXY-2-PHENYL-BENZOFURAN-3-CARBOXYLIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Ethyl5-hydroxy-2-phenylbenzofuran-3-carboxylate
25mg
$ 50.00

Crysdot
Ethyl5-hydroxy-2-phenylbenzofuran-3-carboxylate 97%
1g
$ 301.00

American Custom Chemicals Corporation
5-HYDROXY-2-PHENYL-BENZOFURAN-3-CARBOXYLIC ACID ETHYL ESTER 95.00%
2.5G
$ 1119.71

American Custom Chemicals Corporation
5-HYDROXY-2-PHENYL-BENZOFURAN-3-CARBOXYLIC ACID ETHYL ESTER 95.00%
1G
$ 794.34

AK Scientific
5-Hydroxy-2-phenyl-benzofuran-3-carboxylicacidethylester
1g
$ 730.00

Total 8 raw suppliers

Chemical Property of 5-HYDROXY-2-PHENYL-BENZOFURAN-3-CARBOXYLIC ACID ETHYL ESTER

Chemical Property:

Vapor Pressure:1.67E-09mmHg at 25°C
Melting Point:154-155 °C(Solv: acetic acid (64-19-7))
Boiling Point:471.3°C at 760 mmHg
PKA:8.34±0.40(Predicted)
Flash Point:238.8°C
PSA：59.67000
Density:1.257g/cm³
LogP:3.98210

Purity/Quality:

99%, ^*data from raw suppliers

Ethyl5-hydroxy-2-phenylbenzofuran-3-carboxylate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-HYDROXY-2-PHENYL-BENZOFURAN-3-CARBOXYLIC ACID ETHYL ESTER

There total 6 articles about 5-HYDROXY-2-PHENYL-BENZOFURAN-3-CARBOXYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 106-51-4
p-benzoquinone

: 4610-75-7
5-hydroxyl‐2‐phenylbenzofuran-3-carboxylate ethyl ester

Guidance literature:: With bismuth(III) chloride; In toluene; for 8h; regioselective reaction; Inert atmosphere; Reflux;

Reference yield: 63.0%

: 1174758-95-2
ethyl 5-hydroxy-2-(methylthio)benzofuran-3-carboxylate

: 98-80-6
phenylboronic acid

: 4610-75-7
5-hydroxyl‐2‐phenylbenzofuran-3-carboxylate ethyl ester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; In 1,4-dioxane; at 90 ℃; for 8h; Temperature; Time; Solvent; Inert atmosphere;
DOI:10.1021/jo400984h

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 4610-75-7
5-hydroxyl‐2‐phenylbenzofuran-3-carboxylate ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium bromate

2: zinc(II) chloride / toluene / 12.25 h / 70 - 140 °C / Dean-Stark

With potassium bromate; zinc(II) chloride; In toluene;
DOI:10.1016/j.bmcl.2014.03.087