Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[4-methyl-

Base Information

Chemical Name:Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[4-methyl-
CAS No.:47771-56-2
Molecular Formula:C27H35N3O4S2
Molecular Weight:529.725
Hs Code.:

Synonyms:N,N'-bis(4-methylbenzenesulfonyl)bis(3-aminopropyl)benzylamine;N-benzylbis(3-toluenesulfonamidopropyl)amine;N,N'-bis(p-toluenesulfonyl)bis(3-aminopropyl)benzylamine;N,N-bis(3-tosylaminopropyl)benzylamine;

Suppliers and Price of Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[4-methyl-

Chemical Property:

PSA：112.34000
LogP:6.78600

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[4-methyl-

There total 10 articles about Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 3245-95-2
N-(3-bromo-propyl)-4-methyl-benzenesulfonamide

: 100-46-9
benzylamine

: 47771-56-2
N⁴-benzyl-N¹,N⁷-ditosyl-4-aza-1,7-heptanediamine

Guidance literature:: With sodium hydrogencarbonate; In acetonitrile; at 70 ℃; for 70h;
DOI:10.1246/bcsj.73.693

Reference yield: 95.0%

: 1555-71-1
N1-(3-amino-propyl)-N1-benzyl-propane-1,3-diamine

: 98-59-9
p-toluenesulfonyl chloride

: 47771-56-2
N⁴-benzyl-N¹,N⁷-ditosyl-4-aza-1,7-heptanediamine

Guidance literature:: With sodium hydroxide; In dichloromethane; water; for 3h;

Reference yield:

: 111-94-4
3,3'-Iminodipropionitrile

: 47771-56-2
N⁴-benzyl-N¹,N⁷-ditosyl-4-aza-1,7-heptanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / NaI; Na₂CO₃ / acetonitrile / 5 h / Heating

2: 81 percent / aq. NaOH; H₂ / Raney Ni / ethanol / 48 h / 1034.3 - 1551.44 Torr

3: aq. NaOH; NaCl / diethyl ether / 12 h / 20 °C

With sodium hydroxide; hydrogen; sodium carbonate; sodium iodide; sodium chloride; nickel; In diethyl ether; ethanol; acetonitrile;
DOI:10.1021/jm0582524