4-(3-(1,3-Benzodioxol-5-yl)-1-oxo-2-propenyl)morpholine

Base Information

Chemical Name:4-(3-(1,3-Benzodioxol-5-yl)-1-oxo-2-propenyl)morpholine
CAS No.:74957-53-2
Molecular Formula:C₁₄H₁₅NO₄
Molecular Weight:261.277
Hs Code.:
Metabolomics Workbench ID:122693
ChEMBL ID:CHEMBL118703

Synonyms:4-(3-(1,3-Benzodioxol-5-yl)-1-oxo-2-propenyl)morpholine;CHEMBL118703;74957-53-2;Morpholine, 4-(3-(1,3-benzodioxol-5-yl)-1-oxo-2-propenyl)-;MLS000562661;3-Benzo[1,3]dioxol-5-yl-1-morpholin-4-yl-propenone;SCHEMBL20866523;HMS2330K17;BDBM50401985;STK416912;AKOS000536036;NCGC00245485-01;SMR000175479;AB00083056-01;Z31721639;(2E)-3-(1,3-benzodioxol-5-yl)-1-(morpholin-4-yl)prop-2-en-1-one

Suppliers and Price of 4-(3-(1,3-Benzodioxol-5-yl)-1-oxo-2-propenyl)morpholine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 4-(3-(1,3-Benzodioxol-5-yl)-1-oxo-2-propenyl)morpholine

Chemical Property:

Vapor Pressure:1.58E-09mmHg at 25°C
Boiling Point:484.1°C at 760 mmHg
Flash Point:246.6°C
Density:1.307g/cm³
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:261.10010796
Heavy Atom Count:19
Complexity:351

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCN1C(=O)C=CC2=CC3=C(C=C2)OCO3
Isomeric SMILES:C1COCCN1C(=O)/C=C/C2=CC3=C(C=C2)OCO3

Technology Process of 4-(3-(1,3-Benzodioxol-5-yl)-1-oxo-2-propenyl)morpholine

There total 2 articles about 4-(3-(1,3-Benzodioxol-5-yl)-1-oxo-2-propenyl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 96249-87-5,26930-49-4
3-benzo[1,3]dioxol-5-yl-acryloyl chloride

: 74957-53-2
5363077

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1039/c7ra00408g

Reference yield:

: 2373-80-0,38489-76-8
3,4-(methylenedioxy)cinnamic acid

: 74957-53-2
5363077

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / tetrahydrofuran / 6 h / Inert atmosphere; Cooling with ice

2: triethylamine / dichloromethane / 20 °C

With oxalyl dichloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c7ra00408g