Benzene, 1-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy) phenyl]ethenyl]phenyl]ethenyl]-4-[(1E)-2-(4-isocyanatophenyl)ethenyl]-2, 5-bis[(2S)-2-methylbutoxy]-

Base Information

• Chemical Name: Benzene, 1-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy) phenyl]ethenyl]phenyl]ethenyl]-4-[(1E)-2-(4-isocyanatophenyl)ethenyl]-2, 5-bis[(2S)-2-methylbutoxy]-
• CAS No.: 479579-95-8
• Molecular Formula: C₈₇H₁₃₅NO₈
• Molecular Weight: 1323.03
• Mol file: 479579-95-8.mol

Synonyms:

Chemical Property of Benzene, 1-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy) phenyl]ethenyl]phenyl]ethenyl]-4-[(1E)-2-(4-isocyanatophenyl)ethenyl]-2, 5-bis[(2S)-2-methylbutoxy]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzene, 1-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy) phenyl]ethenyl]phenyl]ethenyl]-4-[(1E)-2-(4-isocyanatophenyl)ethenyl]-2, 5-bis[(2S)-2-methylbutoxy]-

There total 2 articles about Benzene, 1-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy) phenyl]ethenyl]phenyl]ethenyl]-4-[(1E)-2-(4-isocyanatophenyl)ethenyl]-2, 5-bis[(2S)-2-methylbutoxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosgene (75-44-5) + (E,E,E)-4-{4-[4-(3,4,5-tridodecyloxystyryl)-2,5-bis[(S)-2-methylbutoxy]styryl]-2,5-bis[(S)-2-methylbutoxy]styryl}aniline (479579-94-7) → (E,E,E)-4-{4-[4-(3,4,5-tridodecyloxystyryl)-2,5-bis[(S)-2-methylbutoxy]styryl]-2,5-bis[(S)-2-methylbutoxy]styryl} phenyl isocyanate (479579-95-8)

Guidance literature:

In toluene; at 95 ℃; for 15h;

DOI:10.1002/1521-3765(20020802)8:15<3353::AID-CHEM3353>3.0.CO;2-X

Reference yield:

C86H135NO9 → (E,E,E)-4-{4-[4-(3,4,5-tridodecyloxystyryl)-2,5-bis[(S)-2-methylbutoxy]styryl]-2,5-bis[(S)-2-methylbutoxy]styryl} phenyl isocyanate (479579-95-8)

Guidance literature:

Multi-step reaction with 2 steps

1: SnCl₂*2H₂O

2: toluene / 15 h / 95 °C

With tin(ll) chloride; In toluene;

DOI:10.1002/1521-3765(20020802)8:15<3353::AID-CHEM3353>3.0.CO;2-X

upstream raw materials:

phosgene

(E,E,E)-4-{4-[4-(3,4,5-tridodecyloxystyryl)-2,5-bis[(S)-2-methylbutoxy]styryl]-2,5-bis[(S)-2-methylbutoxy]styryl}aniline