Technology Process of 2-FLUORO-BENZENE-1,4-DIAMINE
There total 4 articles about 2-FLUORO-BENZENE-1,4-DIAMINE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium chloride; zinc;
In
ethanol; water;
at 25 ℃;
for 2h;
Inert atmosphere;
- Guidance literature:
-
With
[Cu2(2,7-bis(pyridin-2-yl)-l,8-naphthyridine)(OH)(CF3COO)3]; tetrabutylammomium bromide; ammonia; caesium carbonate;
In
ethylene glycol;
at 140 ℃;
for 16h;
chemoselective reaction;
Sealed tube;
DOI:10.1016/j.catcom.2012.11.027
- Guidance literature:
-
With
silver tetrafluoroborate; 4,4'-Dimethoxy-2,2'-bipyridin; potassium tert-butylate; hydrogen;
In
1,4-dioxane;
at 80 ℃;
for 24h;
under 30003 Torr;
Autoclave;