Benzaldehyde, 2-bromo-4,5-bis(phenylmethoxy)-

Base Information

Chemical Name:Benzaldehyde, 2-bromo-4,5-bis(phenylmethoxy)-
CAS No.:4816-00-6
Molecular Formula:C21H17BrO3
Molecular Weight:397.268
Hs Code.:
DSSTox Substance ID:DTXSID70461467
Wikidata:Q82285821
Mol file:4816-00-6.mol

Synonyms:Benzaldehyde, 2-bromo-4,5-bis(phenylmethoxy)-;4816-00-6;4,5-Bis(benzyloxy)-2-bromobenzaldehyde;2-bromo-4,5-bis(phenylmethoxy)benzaldehyde;DTXSID70461467;CS-0227515;F83125

Suppliers and Price of Benzaldehyde, 2-bromo-4,5-bis(phenylmethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Benzaldehyde, 2-bromo-4,5-bis(phenylmethoxy)-

Chemical Property:

XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:396.03611
Heavy Atom Count:25
Complexity:391

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC2=C(C=C(C(=C2)C=O)Br)OCC3=CC=CC=C3

Technology Process of Benzaldehyde, 2-bromo-4,5-bis(phenylmethoxy)-

There total 7 articles about Benzaldehyde, 2-bromo-4,5-bis(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 4815-99-0
2-bromo-4,5-dihydroxybenzoaldehyde

: 100-39-0
benzyl bromide

: 4816-00-6
3,4-bis(benzyloxy)-6-bromobenzaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Reflux;
DOI:10.1055/s-0031-1290135

Reference yield: 66.0%

: 4815-99-0
2-bromo-4,5-dihydroxybenzoaldehyde

: 100-44-7
benzyl chloride

: 4816-00-6
3,4-bis(benzyloxy)-6-bromobenzaldehyde

Guidance literature:: With potassium carbonate; sodium iodide; In ethanol; for 3h; Heating;

Reference yield:

: 15930-53-7
6-bromo-3,4-methylenedioxybenzaldehyde

: 4816-00-6
3,4-bis(benzyloxy)-6-bromobenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / CH₂Cl₂ / 2 h

2: 6N HCl, KI / tetrahydrofuran / Heating

3: K₂CO₃, KI / ethanol / 18 h / Heating

With hydrogenchloride; aluminium trichloride; potassium carbonate; potassium iodide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo00337a007