2-Aminobenzo[c]cinnoline

Base Information

• Chemical Name: 2-Aminobenzo[c]cinnoline
• CAS No.: 4827-07-0
• Molecular Formula: C12H9N3
• Molecular Weight: 195.22000
• Mol file: 4827-07-0.mol

Synonyms:benzo[c]cinnolin-2-ylamine;Benzo[c]cinnolin-2-ylamin;2-Amino-benzocinnolin;

Chemical Property of 2-Aminobenzo[c]cinnoline

Chemical Property:

• Melting Point: 247 °C (ethanol)
• Boiling Point: 246.6±13.0 °C(Predicted)
• PKA: 4.77±0.30(Predicted)
• PSA: 51.80000
• Density: 1.333±0.06 g/cm3(Predicted)
• LogP: 2.94640

Purity/Quality:

95% ^*data from raw suppliers

Benzo[c]cinnolin-2-amine 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Aminobenzo[c]cinnoline

There total 3 articles about 2-Aminobenzo[c]cinnoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitrobenzocinnoline oxide (70092-61-4) → 2-Amino-benzocinnolin (4827-07-0)

Guidance literature:

With hydrogenchloride; water; tin(ll) chloride;

DOI:10.1039/jr9450000824

Reference yield:

benzo[c]cinnoline-N-oxide (6141-98-6) → 2-Amino-benzocinnolin (4827-07-0)

Guidance literature:

Multi-step reaction with 2 steps

1: HNO₃

2: Raney nickel; ethanol / Hydrogenation

With ethanol; nitric acid; nickel;

DOI:10.1039/jr9450000824

Reference yield:

→ 2-Amino-benzocinnolin (4827-07-0)

Guidance literature:

4-Benzalamino-azobenzol in konz. H2SO4 unter UV-Bestrahlung;

upstream raw materials:

2-nitrobenzocinnoline oxide

benzo[c]cinnoline-N-oxide

Downstream raw materials:

N-benzo[c]cinnolin-2-yl-N-(2-diethylamino-ethyl)-toluene-4-sulfonamide

N-benzo[c]cinnolin-2-yl-toluene-4-sulfonamide