1-(3-chloro-4-fluorophenyl)-2-(4-nitrophenyl)-1H-imidazo[4,5-b]quinoxaline

Base Information

Chemical Name:1-(3-chloro-4-fluorophenyl)-2-(4-nitrophenyl)-1H-imidazo[4,5-b]quinoxaline
CAS No.:4848-71-9
Molecular Formula:C9H14SeSn
Molecular Weight:319.88
Hs Code.:
DSSTox Substance ID:DTXSID40964071
Wikidata:Q82945989
Mol file:4848-71-9.mol

Synonyms:4848-71-9;1-(3-chloro-4-fluorophenyl)-2-(4-nitrophenyl)-1H-imidazo[4,5-b]quinoxaline;DTXSID40964071;AKOS005531809

Suppliers and Price of 1-(3-chloro-4-fluorophenyl)-2-(4-nitrophenyl)-1H-imidazo[4,5-b]quinoxaline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-(3-chloro-4-fluorophenyl)-2-(4-nitrophenyl)-1H-imidazo[4,5-b]quinoxaline

Chemical Property:

Vapor Pressure:2.07E-17mmHg at 25°C
XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:419.0585305
Heavy Atom Count:30
Complexity:631

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)N=C3C(=N2)N(C(=N3)C4=CC=C(C=C4)[N+](=O)[O-])C5=CC(=C(C=C5)F)Cl

Technology Process of 1-(3-chloro-4-fluorophenyl)-2-(4-nitrophenyl)-1H-imidazo[4,5-b]quinoxaline

There total 6 articles about 1-(3-chloro-4-fluorophenyl)-2-(4-nitrophenyl)-1H-imidazo[4,5-b]quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 33861-17-5
phenyl trimethylsilyl selenide

: 1066-45-1
trimethyltin(IV)chloride

: 4848-71-9
trimethylstannyl phenyl selenide

Guidance literature:: In neat (no solvent);
DOI:10.1039/DT9760001730

Reference yield: 85.0%

: 1666-13-3
diphenyl diselenide

: 1066-45-1
trimethyltin(IV)chloride

: 4848-71-9
trimethylstannyl phenyl selenide

Guidance literature:: With liquid NH₃; Li; In tetrahydrofuran; 100 mL liquid NH3 added to diselenide, to this stirred soln. lithium added until soln. was slightly blue, solvent evaporated under Ar, remaining NH3 removed under vacuum, THF added, soln. of Me3SnCl in THF added at room temp. under Ar, stirred for 3 h; THF removed at normal pressure, product distilled from react. flask, redistilled, aqueous phase treated with ether, washed, dried, solvent removed, product purified by column chromy.;
DOI:10.1002/(SICI)1099-0682(200006)2000:6<1307::AID-EJIC1307>3.3.CO;2-Q