1-(3-Phenyldiazenylphenyl)ethanone

Base Information

Chemical Name:1-(3-Phenyldiazenylphenyl)ethanone
CAS No.:4865-93-4
Molecular Formula:C₁₄H₁₂N₂O
Molecular Weight:224.262
Hs Code.:
DSSTox Substance ID:DTXSID80405211
Nikkaji Number:J1.474.401K
Mol file:4865-93-4.mol

Synonyms:3'-(PHENYLAZO)ACETOPHENONE;4865-93-4;1-(3-phenyldiazenylphenyl)ethanone;DTXSID80405211;AKOS024337296

Suppliers and Price of 1-(3-Phenyldiazenylphenyl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-(3-Phenyldiazenylphenyl)ethanone

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:224.094963011
Heavy Atom Count:17
Complexity:282

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=CC(=CC=C1)N=NC2=CC=CC=C2

Technology Process of 1-(3-Phenyldiazenylphenyl)ethanone

There total 6 articles about 1-(3-Phenyldiazenylphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₁₄H₁₄N₂O

: 4865-93-4,15516-65-1
(E)-1-(3-(phenyldiazenyl)phenyl)ethan-1-one

Guidance literature:: With hydrogen bromide; dihydrogen peroxide; In 1,4-dioxane; water; at 50 ℃; for 0.5h;
DOI:10.1016/j.tet.2021.132546

Reference yield:

: 586-96-9
Nitrosobenzene

: 4865-93-4,15516-65-1
(E)-1-(3-(phenyldiazenyl)phenyl)ethan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / ethanol / 40 °C

2: ammonium chloride; zinc / water; ethanol / 20 °C

3: hydrogen bromide; dihydrogen peroxide / water; 1,4-dioxane / 0.5 h / 50 °C

With hydrogen bromide; dihydrogen peroxide; ammonium chloride; acetic acid; zinc; In 1,4-dioxane; ethanol; water;
DOI:10.1016/j.tet.2021.132546

Reference yield:

: C₁₄H₁₂N₂O

: 4865-93-4,15516-65-1
(E)-1-(3-(phenyldiazenyl)phenyl)ethan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; zinc / water; ethanol / 20 °C

2: hydrogen bromide; dihydrogen peroxide / water; 1,4-dioxane / 0.5 h / 50 °C

With hydrogen bromide; dihydrogen peroxide; ammonium chloride; zinc; In 1,4-dioxane; ethanol; water;
DOI:10.1016/j.tet.2021.132546