4-AMINO-3-METHOXYPHENYLCARBAMIC ACID TERT-BUTYL ESTER

Base Information

• Chemical Name: 4-AMINO-3-METHOXYPHENYLCARBAMIC ACID TERT-BUTYL ESTER
• CAS No.: 487065-22-5
• Molecular Formula: C12H18N2O3
• Molecular Weight: 238.287
• Mol file: 487065-22-5.mol

Synonyms:(4-Amino-3-methoxy-phenyl)-carbamic acid tert-butyl ester;4-amino-3-methoxy-phenyl-carbamic acid tert-butyl ester;tert-butyl 4-amino-3-methoxy-phenyl-carbamate;

Chemical Property of 4-AMINO-3-METHOXYPHENYLCARBAMIC ACID TERT-BUTYL ESTER

Chemical Property:

• PSA: 73.58000
• LogP: 3.27860

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-AMINO-3-METHOXYPHENYLCARBAMIC ACID TERT-BUTYL ESTER

There total 1 articles about 4-AMINO-3-METHOXYPHENYLCARBAMIC ACID TERT-BUTYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl (3-methoxy-4-nitrophenyl)carbamate (877671-39-1) → N-(tert-butoxycarbonyl)-3-methoxy-1,4-phenylenediamine (487065-22-5)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃;

Reference yield:

N-(tert-butoxycarbonyl)-3-methoxy-1,4-phenylenediamine (487065-22-5) + (R)-2-chloro-8-cyclopentyl-7-ethyl-5-methyl-7,8-dihydropteridin-6(5H)-one (755039-55-5) → C26H36N6O4

Guidance literature:

at 120 ℃; for 5h;

Reference yield:

N-(tert-butoxycarbonyl)-3-methoxy-1,4-phenylenediamine (487065-22-5) + C14H21ClN4O (755039-65-7) → C26H38N6O4

Guidance literature:

at 120 ℃; for 4.5h;

upstream raw materials:

tert-butyl (3-methoxy-4-nitrophenyl)carbamate

Downstream raw materials:

1-acetyl-6-amino-8-methoxy-4-phenyl-1,2,3,4-tetrahydro-2,2,4,7-tetramethylquinoline