14-Hydroxy-14-azadispiro[5.1.58.26]pentadec-12-ene-7,15-dione

Base Information

• Chemical Name: 14-Hydroxy-14-azadispiro[5.1.58.26]pentadec-12-ene-7,15-dione
• CAS No.: 4881-20-3
• Molecular Formula: C14H19NO3
• NSC Number: 137362
• DSSTox Substance ID: DTXSID90300506
• Mol file: 4881-20-3.mol

Synonyms:4881-20-3;14-Hydroxy-14-azadispiro[5.1.58.26]pentadec-12-ene-7,15-dione;NSC137362;ST024296;Oprea1_200130;DTXSID90300506;AKOS024278848;NSC-137362

Chemical Property of 14-Hydroxy-14-azadispiro[5.1.58.26]pentadec-12-ene-7,15-dione

Chemical Property:

• Vapor Pressure: 8.88E-10mmHg at 25°C
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 249.13649347
• Heavy Atom Count: 18
• Complexity: 423

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC2(CC1)C(=O)C3(CCCC=C3)N(C2=O)O

Technology Process of 14-Hydroxy-14-azadispiro[5.1.58.26]pentadec-12-ene-7,15-dione

There total 2 articles about 14-Hydroxy-14-azadispiro[5.1.58.26]pentadec-12-ene-7,15-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 14-Hydroxy-14-aza-dispiro<5.1.5.2>pentadec-9-en-7,15-dion (4881-20-3)

Guidance literature:

With sulfuric acid;

DOI:10.1021/jo01096a023

Reference yield:

→ 14-Hydroxy-14-aza-dispiro<5.1.5.2>pentadec-9-en-7,15-dion (4881-20-3)

Guidance literature:

14-Hydroxy-14-aza-dispiro<5.1.5.2>pentadecen-(9)-dion-(7,15)-oxim-(7), konz. HCl, in n-Butanol;

DOI:10.1021/jo01265a074

Reference yield:

14-Hydroxy-14-aza-dispiro<5.1.5.2>pentadec-9-en-7,15-dion (4881-20-3) + methyl iodide (74-88-4) → 14-methoxy-14-aza-dispiro[5.1.5.2]pentadec-9-ene-7,15-dione (88113-43-3)

Guidance literature:

With potassium hydroxide; In acetone; for 0.333333h; Ambient temperature;

Downstream raw materials:

14-methoxy-14-aza-dispiro[5.1.5.2]pentadec-9-ene-7,15-dione

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