3-Methyl-1-adamantaneacetic acid

Base Information

Chemical Name:3-Methyl-1-adamantaneacetic acid
CAS No.:14202-13-2
Molecular Formula:C13H20 O2
Molecular Weight:208.301
Hs Code.:
European Community (EC) Number:238-054-4
DSSTox Substance ID:DTXSID40931304

Synonyms:3-Methyl-1-adamantaneacetic acid;14202-13-2;2-(3-methyl-1-adamantyl)acetic acid;3-methyladamantan-1-ylacetic acid;EINECS 238-054-4;3-Methyltricyclo(3.3.1.13,7)decan-1-ylacetic acid;(3-methyladamantan-1-yl)acetic acid;3-methyltricyclo[3.3.1.13,7]decan-1-ylacetic acid;CBMicro_019139;Tricyclo(3.3.1.1(3,7)-)decane-1-acetic acid, 3-methyl-;Tricyclo[3.3.1.1(3,7)-]decane-1-acetic acid, 3-methyl-;Cambridge id 5357729;Oprea1_266934;SCHEMBL503339;DTXSID40931304;HMS1608I12;(3-Methyl-1-adamantyl)acetic acid;CCG-7258;(3-Methyl-1-adamantyl)acetic acid #;BIM-0018944.P001;AB00082794-01;SR-01000400504;SR-01000400504-1

Suppliers and Price of 3-Methyl-1-adamantaneacetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-Methyl-1-adamantaneacetic acid

Chemical Property:

Vapor Pressure:3.62E-05mmHg at 25°C
Boiling Point:328.9°C at 760 mmHg
Flash Point:164.7°C
Density:1.149g/cm³
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:208.146329876
Heavy Atom Count:15
Complexity:294

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC12CC3CC(C1)CC(C3)(C2)CC(=O)O

Technology Process of 3-Methyl-1-adamantaneacetic acid

There total 12 articles about 3-Methyl-1-adamantaneacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 75-35-4,9002-85-1
1,1-Dichloroethylene

: 702-81-8
3-methyl-1-adamantanol

: 14202-13-2
(3-methyladamantan-1-yl)acetic acid

Guidance literature:: 1,1-Dichloroethylene; 3-methyl-1-adamantanol; With sulfuric acid; In dichloromethane; at 0 - 30 ℃;

With water; In dichloromethane; at 0 ℃;
DOI:10.1134/S1070428017080024

Reference yield: 82.6%

: 75-35-4,9002-85-1
1,1-Dichloroethylene

: 101974-65-6
3-methyl-1-adamantanol nitrate

: 14202-13-2
(3-methyladamantan-1-yl)acetic acid

Guidance literature:: With sulfuric acid; for 1h;
DOI:10.1007/BF00953951

Reference yield:

: 702-77-2
1-bromo-3-methyladamantane

: 14202-13-2
(3-methyladamantan-1-yl)acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: H₂SO₄

2: H₂SO₄

3: LiAlH₄

4: HBr / acetic acid

5: (i) Mg, (ii) /BRN= 1900390/

With lithium aluminium tetrahydride; sulfuric acid; hydrogen bromide; In acetic acid;