7-Bromo-6-methoxy-2-methyl-5,8-quinolinedione

Base Information

Chemical Name:7-Bromo-6-methoxy-2-methyl-5,8-quinolinedione
CAS No.:61895-37-2
Molecular Formula:C11H8BrNO3
Molecular Weight:282.0901
Hs Code.:
NSC Number:132492
UNII:39B2676EQC
DSSTox Substance ID:DTXSID80210908
Wikidata:Q83085740
ChEMBL ID:CHEMBL1707222

Synonyms:61895-37-2;7-Bromo-6-methoxy-2-methyl-5,8-quinolinedione;7-bromo-6-methoxy-2-methylquinoline-5,8-dione;MLS002920162;NSC132492;39B2676EQC;NSC-132492;SMR001797759;NSC 132492;UNII-39B2676EQC;cid_280615;CHEMBL1707222;BDBM81271;DTXSID80210908;NCI60_000717;7-bromo-6-methoxy-2-methyl-quinoline-5,8-dione;5,8-Quinolinedione, 7-bromo-6-methoxy-2-methyl-;7-bromanyl-6-methoxy-2-methyl-quinoline-5,8-dione;7-bromo-6-methoxy-2-methyl-quinoline-5,8-quinone

Suppliers and Price of 7-Bromo-6-methoxy-2-methyl-5,8-quinolinedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 7-Bromo-6-methoxy-2-methyl-5,8-quinolinedione

Chemical Property:

Vapor Pressure:5.31E-07mmHg at 25°C
Boiling Point:412.1°C at 760 mmHg
Flash Point:203°C
Density:1.67g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:280.96876
Heavy Atom Count:16
Complexity:377

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC2=C(C=C1)C(=O)C(=C(C2=O)Br)OC

Technology Process of 7-Bromo-6-methoxy-2-methyl-5,8-quinolinedione

There total 5 articles about 7-Bromo-6-methoxy-2-methyl-5,8-quinolinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 30831-32-4
6-methoxy-2-methylquinoline-5,8-dione

: 61895-37-2
7-Brom-6-methoxy-2-methyl-5,8-chinolindion

Guidance literature:: With bromine; sodium acetate; acetic acid; at 20 ℃; for 24h;
DOI:10.1021/ol035381a

Reference yield:

: 61895-33-8
5,8-Dinitro-6-methoxy-2-methylchinolin

: 61895-37-2
7-Brom-6-methoxy-2-methyl-5,8-chinolindion

Guidance literature:: Multi-step reaction with 3 steps

1: H₂; HCl / Pd/C / H₂O / 24 h / 20 °C / 2068.59 Torr

2: FeCl₃ / CHCl₃; H₂O / 24 h / 20 °C

3: 86 percent / Br₂; HOAc; NaOAc / 24 h / 20 °C

With hydrogenchloride; hydrogen; bromine; sodium acetate; iron(III) chloride; acetic acid; palladium on activated charcoal; In chloroform; water;
DOI:10.1021/ol035381a

Reference yield:

: 54232-06-3
6-methoxy-2-methyl-8-nitroquinoline

: 61895-37-2
7-Brom-6-methoxy-2-methyl-5,8-chinolindion

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / HNO₃; H₂SO₄ / 3 h / 20 °C

2: H₂; HCl / Pd/C / H₂O / 24 h / 20 °C / 2068.59 Torr

3: FeCl₃ / CHCl₃; H₂O / 24 h / 20 °C

4: 86 percent / Br₂; HOAc; NaOAc / 24 h / 20 °C

With hydrogenchloride; sulfuric acid; hydrogen; bromine; nitric acid; sodium acetate; iron(III) chloride; acetic acid; palladium on activated charcoal; In chloroform; water;
DOI:10.1021/ol035381a