5,8-Dinitro-6-methoxyquinaldine

Base Information

Chemical Name:5,8-Dinitro-6-methoxyquinaldine
CAS No.:61895-33-8
Molecular Formula:C11H9N3O5
Molecular Weight:263.21
Hs Code.:2933499090
NSC Number:101647
DSSTox Substance ID:DTXSID20210907
Nikkaji Number:J73.000I
Wikidata:Q83085738
ChEMBL ID:CHEMBL1869668

Synonyms:5,8-Dinitro-6-methoxyquinaldine;61895-33-8;Quinaldine, 5,8-dinitro-6-methoxy-;MLS002703654;BRN 1491003;Quinoline, 2-methyl-6-methoxy-5,8-dinitro-;NSC101647;NCIOpen2_006913;5-21-03-00340 (Beilstein Handbook Reference);CHEMBL1869668;DTXSID20210907;Quinaldine,8-dinitro-6-methoxy-;NSC 101647;NSC-101647;SMR001570371

Suppliers and Price of 5,8-Dinitro-6-methoxyquinaldine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
6-METHOXY-2-METHYL-5,8-DINITROQUINOLINE 95.00%
5MG
$ 505.86

Total 4 raw suppliers

Chemical Property of 5,8-Dinitro-6-methoxyquinaldine

Chemical Property:

Vapor Pressure:5.91E-08mmHg at 25°C
Boiling Point:452.7°C at 760 mmHg
Flash Point:227.6°C
PSA：113.76000
Density:1.456g/cm³
LogP:3.41460
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:1
Exact Mass:263.05422040
Heavy Atom Count:19
Complexity:366

Purity/Quality:

99% ^*data from raw suppliers

6-METHOXY-2-METHYL-5,8-DINITROQUINOLINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC2=C(C=C1)C(=C(C=C2[N+](=O)[O-])OC)[N+](=O)[O-]

Technology Process of 5,8-Dinitro-6-methoxyquinaldine

There total 2 articles about 5,8-Dinitro-6-methoxyquinaldine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 54232-06-3
6-methoxy-2-methyl-8-nitroquinoline

: 61895-33-8
5,8-Dinitro-6-methoxy-2-methylchinolin

Guidance literature:: With sulfuric acid; nitric acid; at 20 ℃; for 3h;
DOI:10.1021/ol035381a

Reference yield:

: 61895-33-8
5,8-Dinitro-6-methoxy-2-methylchinolin

Guidance literature:: 3c, rauch. HNO3, konz. H2SO4;
DOI:10.1002/jhet.5570130525

Reference yield:

: 61895-33-8
5,8-Dinitro-6-methoxy-2-methylchinolin

: 61895-37-2
7-Brom-6-methoxy-2-methyl-5,8-chinolindion

Guidance literature:: Multi-step reaction with 3 steps

1: H₂; HCl / Pd/C / H₂O / 24 h / 20 °C / 2068.59 Torr

2: FeCl₃ / CHCl₃; H₂O / 24 h / 20 °C

3: 86 percent / Br₂; HOAc; NaOAc / 24 h / 20 °C

With hydrogenchloride; hydrogen; bromine; sodium acetate; iron(III) chloride; acetic acid; palladium on activated charcoal; In chloroform; water;
DOI:10.1021/ol035381a