Carbamic acid, [4-[3-[4-[[(1,1-dimethylethoxy)carbonyl](phenylmethoxy)amino]butyl]tetra hydro-2,4,6-trioxo-1,3,5-triazin-1(2H)-yl]butyl](phenylmethoxy)-, 2,2,2-trichloroethyl ester

Base Information

Chemical Name:Carbamic acid, [4-[3-[4-[[(1,1-dimethylethoxy)carbonyl](phenylmethoxy)amino]butyl]tetra hydro-2,4,6-trioxo-1,3,5-triazin-1(2H)-yl]butyl](phenylmethoxy)-, 2,2,2-trichloroethyl ester
CAS No.:489453-01-2
Molecular Formula:C33H42Cl3N5O9
Molecular Weight:759.084
Hs Code.:
Mol file:489453-01-2.mol

Carbamic acid,
[4-[3-[4-[[(1,1-dimethylethoxy)carbonyl](phenylmethoxy)amino]butyl]tetra
hydro-2,4,6-trioxo-1,3,5-triazin-1(2H)-yl]butyl](phenylmethoxy)-,
2,2,2-trichloroethyl ester

Synonyms:

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Chemical Property of Carbamic acid, [4-[3-[4-[[(1,1-dimethylethoxy)carbonyl](phenylmethoxy)amino]butyl]tetra hydro-2,4,6-trioxo-1,3,5-triazin-1(2H)-yl]butyl](phenylmethoxy)-, 2,2,2-trichloroethyl ester

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Technology Process of Carbamic acid, [4-[3-[4-[[(1,1-dimethylethoxy)carbonyl](phenylmethoxy)amino]butyl]tetra hydro-2,4,6-trioxo-1,3,5-triazin-1(2H)-yl]butyl](phenylmethoxy)-, 2,2,2-trichloroethyl ester

There total 8 articles about Carbamic acid, [4-[3-[4-[[(1,1-dimethylethoxy)carbonyl](phenylmethoxy)amino]butyl]tetra hydro-2,4,6-trioxo-1,3,5-triazin-1(2H)-yl]butyl](phenylmethoxy)-, 2,2,2-trichloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 27738-96-1
chlorocarbonyl isocyanate

: 489452-98-4
1-[4-[N-(trichloroethoxycarbonyl)benzyloxyamino]butyl]-3-[4-[N-(tert-butyloxycarbonyl)benzyloxyamino]butyl]urea

: 489453-01-2
1-[4-[N-(trichloroethoxycarbonyl)benzyloxyamino]butyl]-3-[4-[N-(tert-butyloxycarbonyl)benzyloxyamino]butyl][1.3.5]triazinane-2,4,6-trione

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1021/jo026391c

Reference yield:

: 79722-21-7
tert-butyl N-(benzyloxy)carbamate

: 489453-01-2
1-[4-[N-(trichloroethoxycarbonyl)benzyloxyamino]butyl]-3-[4-[N-(tert-butyloxycarbonyl)benzyloxyamino]butyl][1.3.5]triazinane-2,4,6-trione

Guidance literature:: Multi-step reaction with 4 steps

1.1: 80 percent / NaH; NaI / dimethylformamide / 5 h / 60 - 70 °C

2.1: ammonium hydroxide; ammonia / Raney 2800 nickel / methanol; H₂O / 0.33 h / 0 - 5 °C

2.2: H₂ / Raney nickel / methanol / 5 h / 2327.23 Torr

3.1: 2.5360 g / toluene / 8 h

4.1: 90 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 - 20 °C

With 2,6-dimethylpyridine; ammonium hydroxide; ammonia; sodium hydride; sodium iodide; Raney 2800 nickel; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo026391c

Reference yield:

: 489452-95-1
4-[N-(tert-butyloxycarbonyl)benzyloxyamino]butyronitrile

: 489453-01-2
1-[4-[N-(trichloroethoxycarbonyl)benzyloxyamino]butyl]-3-[4-[N-(tert-butyloxycarbonyl)benzyloxyamino]butyl][1.3.5]triazinane-2,4,6-trione

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium hydroxide; ammonia / Raney 2800 nickel / methanol; H₂O / 0.33 h / 0 - 5 °C

1.2: H₂ / Raney nickel / methanol / 5 h / 2327.23 Torr

2.1: 2.5360 g / toluene / 8 h

3.1: 90 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 - 20 °C

With 2,6-dimethylpyridine; ammonium hydroxide; ammonia; Raney 2800 nickel; In methanol; dichloromethane; water; toluene;
DOI:10.1021/jo026391c